2-[2-(2-amino-6-methoxy-9H-purin-9-yl)ethyl]propane-1,3-diol

Base Information

Chemical Name:2-[2-(2-amino-6-methoxy-9H-purin-9-yl)ethyl]propane-1,3-diol
CAS No.:97845-65-3
Molecular Formula:C11H17N5O3
Molecular Weight:267.288
Hs Code.:

Synonyms:1,3-Propanediol,2-(2-(2-amino-6-methoxy-9H-purin-9-yl)ethyl);2-amino-6-methoxy-9-(4-hydroxy-3-hydroxymethylbutyl)purine;2-Amino-6-methoxy-9-(4-hydroxy-3-hydroxymethylbut-1-yl)purine;2-amino-9-<4-hydroxy-3-(hydroxymethyl)but-1-yl>-6-methoxypurine;

Suppliers and Price of 2-[2-(2-amino-6-methoxy-9H-purin-9-yl)ethyl]propane-1,3-diol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 4 raw suppliers

Chemical Property of 2-[2-(2-amino-6-methoxy-9H-purin-9-yl)ethyl]propane-1,3-diol

Chemical Property:

Vapor Pressure:5.84E-16mmHg at 25°C
Boiling Point:614.6°Cat760mmHg
Flash Point:325.5°C
PSA：120.04000
Density:1.53g/cm³
LogP:-0.66190

Purity/Quality:: 95%+ or 98%+ ^*data from raw suppliers

Safty Information:

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Technology Process of 2-[2-(2-amino-6-methoxy-9H-purin-9-yl)ethyl]propane-1,3-diol

There total 1 articles about 2-[2-(2-amino-6-methoxy-9H-purin-9-yl)ethyl]propane-1,3-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6482-32-2
2-(hydroxymethyl)butane-1,4-diol

: 97845-65-3
2-amino-9-<4-hydroxy-3-(hydroxymethyl)but-1-yl>-6-methoxypurine

Guidance literature:: Multi-step reaction with 5 steps

1: 41 percent / p-TsOH*H₂O / tetrahydrofuran / 0.5 h / Ambient temperature

2: 87 percent / CBr₄, PPh₃ / dimethylformamide / 0.5 h / 0 °C

3: 64 percent / K₂CO₃ / dimethylformamide / 5 h / Ambient temperature

5: aq. HCl / Ambient temperature

With hydrogenchloride; carbon tetrabromide; potassium carbonate; toluene-4-sulfonic acid; triphenylphosphine; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jm00392a020