Benzenepropanoic acid, 2-methoxy-b-(triphenylgermyl)-

Base Information

Chemical Name:Benzenepropanoic acid, 2-methoxy-b-(triphenylgermyl)-
CAS No.:146139-08-4
Molecular Formula:C₂₈H₂₆GeO₃
Molecular Weight:483.103
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenepropanoic acid, 2-methoxy-b-(triphenylgermyl)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
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MSDS Files:: SDS file from LookChem

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Technology Process of Benzenepropanoic acid, 2-methoxy-b-(triphenylgermyl)-

There total 1 articles about Benzenepropanoic acid, 2-methoxy-b-(triphenylgermyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 136026-02-3
Cl₃GeCH(C₆H₄OCH₃)CH₂COOH

: 100-58-3
phenylmagnesium bromide

: 146139-08-4
Ph₃GeCH(o-CH₃OC₆H₄)CH₂COOH

Guidance literature:: In tetrahydrofuran; Mg-compd. added dropwise at 0°C to Ge-compd. in THF, refluxed for4 h, cooled; 10% aq. HCl added, extracted with CHCl3, CHCl3 phase dried over anhydrous MgSO4, filtered, solv. removed in vac., recrystallised from CHCl3 and acetone (3:1);
DOI:10.1080/15533170701301470

Reference yield: 75.0%

: 146139-08-4
Ph₃GeCH(o-CH₃OC₆H₄)CH₂COOH

: 13356-08-6,12684-28-5
fenbutatin oxide

: 341511-25-9
(C₆H₅)3GeCH(C₆H₄OCH₃)CH₂COOSn(CH₂C(CH₃)2C₆H₅)3

Guidance literature:: In toluene; byproducts: H2O; refluxing a mixt of germanium and tin compds. in toluene for 6 h with a Dean-Stark apparatus, cooling; evapn., drying in vac., recrystn. (CHCl3/petroleum ether); elem. anal.;
DOI:10.1016/S0022-328X(00)00542-8

Reference yield: 64.0%

: 146139-08-4
Ph₃GeCH(o-CH₃OC₆H₄)CH₂COOH

: 60043-16-5
tri(p-tolyl)antimony dibromide

: 945655-57-2
[Ph₃GeCH(o-CH₃OC₆H₄)CH₂COO]2(antimony)(p-CH₃C₆H₄)3

Guidance literature:: With NEt₃; In toluene; byproducts: Et3N*HCl; according to reported method: Ma, Y.Q., Li, J.S. Main Group Met. Chem. 2001, 24, 235-238.; crystd. from CH2Cl2/petroleum ether; elem. anal.;
DOI:10.1080/15533170600862903