1-Cyclohexyl-3-methylbut-2-en-1-one

Base Information

Chemical Name:1-Cyclohexyl-3-methylbut-2-en-1-one
CAS No.:14618-93-0
Molecular Formula:C₁₁H₁₈O
Molecular Weight:166.263
Hs Code.:
DSSTox Substance ID:DTXSID30551939
Nikkaji Number:J3.000.798K
Mol file:14618-93-0.mol

Synonyms:1-Cyclohexyl-3-methylbut-2-en-1-one;14618-93-0;SCHEMBL17156515;DTXSID30551939;AKOS017740995

Suppliers and Price of 1-Cyclohexyl-3-methylbut-2-en-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-Cyclohexyl-3-methylbut-2-en-1-one

Chemical Property:

XLogP3:3.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:166.135765193
Heavy Atom Count:12
Complexity:181

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=CC(=O)C1CCCCC1)C

Technology Process of 1-Cyclohexyl-3-methylbut-2-en-1-one

There total 5 articles about 1-Cyclohexyl-3-methylbut-2-en-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4-cyclohexyl-2,6-dimethyl-1,6-heptadien-4-ol

: 14618-93-0
1-cyclohexyl-3-methyl-2-buten-1-one

: 1-cyclohexyl-3-methyl-3-buten-1-one

Guidance literature:: With potassium hydride; In N,N,N,N,N,N-hexamethylphosphoric triamide; at 80 ℃; Yield given. Yields of byproduct given;
DOI:10.1002/hlca.19870700721

Reference yield:

: 4630-82-4
methyl cyclohexylcarboxylate

: 14618-93-0
1-cyclohexyl-3-methyl-2-buten-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / Mg / tetrahydrofuran / Heating

2: KH / hexamethylphosphoric acid triamide / 80 °C

With potassium hydride; magnesium; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide;
DOI:10.1002/hlca.19870700721