3,4,4-TRIMETHYLPENTANOIC ACID

Base Information

Chemical Name:3,4,4-TRIMETHYLPENTANOIC ACID
CAS No.:75177-71-8
Molecular Formula:C8H16 O2
Molecular Weight:144.214
Hs Code.:
Mol file:75177-71-8.mol

Synonyms:(?à)-3,4,4-Trimethylpentanoic acid;3,4,4-Trimethylpentanoic acid

Suppliers and Price of 3,4,4-TRIMETHYLPENTANOIC ACID

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
3,4,4-trimethylpentanoicacid
50mg
$ 200.00

American Custom Chemicals Corporation
3,4,4-TRIMETHYL PENTANOIC ACID 95.00%
5MG
$ 505.67

AK Scientific
3,4,4-Trimethylpentanoicacid
1g
$ 947.00

AK Scientific
3,4,4-Trimethylpentanoicacid
500mg
$ 760.00

Total 6 raw suppliers

Chemical Property of 3,4,4-TRIMETHYLPENTANOIC ACID

Chemical Property:

Vapor Pressure:0.0348mmHg at 25°C
Boiling Point:223.8°C at 760 mmHg
Flash Point:99.4°C
PSA：37.30000
Density:0.926g/cm³
LogP:2.14330

Purity/Quality:

97% ^*data from raw suppliers

3,4,4-trimethylpentanoicacid ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3,4,4-TRIMETHYLPENTANOIC ACID

There total 1 articles about 3,4,4-TRIMETHYLPENTANOIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 107-93-7
(E)-but-2-enoic acid

: 594-19-4
tert.-butyl lithium

: 625-38-7
but-3-enoic acid

: 75177-71-8
3,4,4-trimethylpentanoic acid

Guidance literature:: In tetrahydrofuran; at -70 ℃; for 2h;
DOI:10.1016/S0040-4020(98)01073-4

Reference yield:

: 75177-71-8
3,4,4-trimethylpentanoic acid

: benzyl 2-phthalimido-3,4,4-trimethyl-pentanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) CsOH / 1.) H₂O, EtOH, 0 deg C, 2.) DMF, 3 h

2: 1.) KHMDS, trisyl azide, 2.) PPh₃ / 1.) toluene, THF, -78 deg C, 1 min, 2.) H₂O, THF, RT, 4 d, then 50 deg C, 2 h

3: 1.) thionyl chloride, DMF, 3.) Et₃N / 1.) reflux, 1 h, 2.) benzene, 3.) THF, 2 h

With cesium hydroxide; thionyl chloride; 2,4,6-Triisopropylbenzenesulfonyl azide; potassium hexamethylsilazane; triethylamine; N,N-dimethyl-formamide; triphenylphosphine;
DOI:10.1016/S0040-4020(01)85232-7

Reference yield:

: 75177-71-8
3,4,4-trimethylpentanoic acid

: benzyl 2-azido-3,4,4-trimethyl-pentanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) CsOH / 1.) H₂O, EtOH, 0 deg C, 2.) DMF, 3 h

2: KHMDS, trisyl azide / toluene; tetrahydrofuran / 0.02 h / -78 °C

With cesium hydroxide; 2,4,6-Triisopropylbenzenesulfonyl azide; potassium hexamethylsilazane; In tetrahydrofuran; toluene;
DOI:10.1016/S0040-4020(01)85232-7