2-[2-(2-Bromophenyl)ethyl]-3,3-dimethylcyclohexan-1-one

Base Information

Chemical Name:2-[2-(2-Bromophenyl)ethyl]-3,3-dimethylcyclohexan-1-one
CAS No.:150270-95-4
Molecular Formula:C16H21BrO
Molecular Weight:309.246
Hs Code.:
DSSTox Substance ID:DTXSID90566246
Mol file:150270-95-4.mol

Synonyms:150270-95-4;2-[2-(2-Bromophenyl)ethyl]-3,3-dimethylcyclohexan-1-one;DTXSID90566246

Suppliers and Price of 2-[2-(2-Bromophenyl)ethyl]-3,3-dimethylcyclohexan-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-[2-(2-Bromophenyl)ethyl]-3,3-dimethylcyclohexan-1-one

Chemical Property:

XLogP3:4.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:308.07758
Heavy Atom Count:18
Complexity:298

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1(CCCC(=O)C1CCC2=CC=CC=C2Br)C

Technology Process of 2-[2-(2-Bromophenyl)ethyl]-3,3-dimethylcyclohexan-1-one

There total 6 articles about 2-[2-(2-Bromophenyl)ethyl]-3,3-dimethylcyclohexan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 150270-94-3
2-<2-(2-Bromophenyl)ethyl>-3-methylcyclohex-2-enone

: 150270-95-4
2-<2-(2-Bromophenyl)ethyl>-3,3-dimethylcyclohexanone

Guidance literature:: With boron trifluoride diethyl etherate;
DOI:10.1039/c39930000809

Reference yield: 84.0%

: 917-54-4
methyllithium

: 150270-94-3
2-<2-(2-Bromophenyl)ethyl>-3-methylcyclohex-2-enone

: 150270-95-4
2-<2-(2-Bromophenyl)ethyl>-3,3-dimethylcyclohexanone

Guidance literature:: With copper(l) iodide; boron trifluoride diethyl etherate; In diethyl ether; 1.) -50 deg C, 5 min, 2.) -30 deg C, 75 min;

Reference yield:

: 487-51-4
4-carbethoxy-3-methyl-2-cyclohexen-1-one

: 150270-95-4
2-<2-(2-Bromophenyl)ethyl>-3,3-dimethylcyclohexanone

Guidance literature:: Multi-step reaction with 3 steps

1: 60 percent / t-BuOK / 2-methyl-propan-2-ol

2: 79 percent / aq. KOH / ethanol / 14 h / Heating

3: 84 percent / CuI, BF₃*Et₂O / diethyl ether / 1.) -50 deg C, 5 min, 2.) -30 deg C, 75 min

With potassium hydroxide; copper(l) iodide; boron trifluoride diethyl etherate; potassium tert-butylate; In diethyl ether; ethanol; tert-butyl alcohol;