2-amino-N-(2-chloropyridin-3-yl)benzamide

Base Information

Chemical Name:2-amino-N-(2-chloropyridin-3-yl)benzamide
CAS No.:956-30-9
Molecular Formula:C12H10 Cl N3 O
Molecular Weight:247.684
Hs Code.:2933399090
European Community (EC) Number:213-478-2
DSSTox Substance ID:DTXSID60241891
Nikkaji Number:J298.563B
Wikidata:Q83125452
Mol file:956-30-9.mol

Synonyms:2-amino-N-(2-chloropyridin-3-yl)benzamide;956-30-9;o-Amino-N-(2-chloro-3-pyridyl)benzamide;2-Amino-N-(2-chloro-pyridin-3-yl)-benzamide;Benzamide, 2-amino-N-(2-chloro-3-pyridinyl)-;EINECS 213-478-2;C12H10ClN3O;Oprea1_227273;SCHEMBL5503426;DTXSID60241891;MFCD01950402;STK824422;AKOS001633463;AB10584;2-chloro-3-(2-aminobenzoyl)aminopyridine;2-Amino-N-(2-chloro-3-pyridyl)benzamide;EU-0007358;SR-01000455515;SR-01000455515-1;F0914-3499

Suppliers and Price of 2-amino-N-(2-chloropyridin-3-yl)benzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
2-AMINO-N-(2-CHLORO-PYRIDIN-3-YL)-BENZAMIDE 95.00%
10G
$ 2638.22

American Custom Chemicals Corporation
2-AMINO-N-(2-CHLORO-PYRIDIN-3-YL)-BENZAMIDE 95.00%
5G
$ 2019.23

American Custom Chemicals Corporation
2-AMINO-N-(2-CHLORO-PYRIDIN-3-YL)-BENZAMIDE 95.00%
1G
$ 1074.98

Total 8 raw suppliers

Chemical Property of 2-amino-N-(2-chloropyridin-3-yl)benzamide

Chemical Property:

Vapor Pressure:3.25E-05mmHg at 25°C
Boiling Point:354.9°Cat760mmHg
Flash Point:168.4°C
PSA：68.01000
Density:1.409g/cm³
LogP:3.22370
XLogP3:2.5
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:247.0512396
Heavy Atom Count:17
Complexity:275

Purity/Quality:

98%min ^*data from raw suppliers

2-AMINO-N-(2-CHLORO-PYRIDIN-3-YL)-BENZAMIDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C(=C1)C(=O)NC2=C(N=CC=C2)Cl)N

Technology Process of 2-amino-N-(2-chloropyridin-3-yl)benzamide

There total 7 articles about 2-amino-N-(2-chloropyridin-3-yl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1028-86-0
N-(2-chloro-pyridin-3-yl)-2-nitro-benzamide

: 956-30-9
2-amino-N-(2-chloropyridin-3-yl)benzamide

Guidance literature:: With iron; ammonium chloride; In ethanol; water; for 0.666667h; Reflux;

Reference yield: 71.0%

: 84446-21-9
3-(2'-chlorobenzoyl)amino-2-chloropyridine

: 956-30-9
2-amino-N-(2-chloropyridin-3-yl)benzamide

Guidance literature:: With ammonium hydroxide; copper(l) chloride; sodium chloride; at 80 ℃; for 3h;

Reference yield:

: 552-16-9,104810-18-6
ortho-nitrobenzoic acid

: 956-30-9
2-amino-N-(2-chloropyridin-3-yl)benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl chloride; DMF / tetrahydrofuran / 1 h / Heating

2: 5.55 g / pyridine / tetrahydrofuran / 2 h / 20 °C

3: 86 percent / aq. HCl; SnCl₂ / 0.25 h / 100 °C

With pyridine; hydrogenchloride; oxalyl dichloride; N,N-dimethyl-formamide; tin(ll) chloride; In tetrahydrofuran;
DOI:10.1021/jm040800a