4-FLUORO-3-METHYLCINNAMIC ACID

Base Information

• Chemical Name: 4-FLUORO-3-METHYLCINNAMIC ACID
• CAS No.: 152152-18-6
• Molecular Formula: C₁₀H₉FO₂
• Molecular Weight: 180.179
• Hs Code.: 2916399090
• Mol file: 152152-18-6.mol

Synonyms:(E)-3-(4-Fluoro-3-methyl-phenyl)-acrylic acid;4-FLUORO-3-METHYLCINNAMIC ACID;

Chemical Property of 4-FLUORO-3-METHYLCINNAMIC ACID

Chemical Property:

• PSA: 37.30000
• LogP: 2.23190

Purity/Quality:

95% ^*data from raw suppliers

4-Fluoro-3-methylcinnamicacid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-FLUORO-3-METHYLCINNAMIC ACID

There total 1 articles about 4-FLUORO-3-METHYLCINNAMIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

malonic acid (141-82-2) + 4-fluoro-3-methylbenzaldehyde (135427-08-6) → 3-methyl-4-fluorocinnamic acid (152152-18-6)

Guidance literature:

With pyridine;

DOI:10.1021/jo034318w

Reference yield:

3-methyl-4-fluorocinnamic acid (152152-18-6) → 3-(4-fluoro-3-methylphenyl)-N-methoxypropionamide (569657-02-9)

Guidance literature:

Multi-step reaction with 3 steps

1: H₂ / Pd/C

With hydrogen; palladium on activated charcoal;

DOI:10.1021/jo034318w

Reference yield:

3-methyl-4-fluorocinnamic acid (152152-18-6) → (E)-3-(4-Fluoro-3-methyl-phenyl)-acryloyl chloride

Guidance literature:

DOI:10.1021/jo034318w

upstream raw materials:

malonic acid

4-fluoro-3-methylbenzaldehyde

Downstream raw materials:

3-(4-fluoro-3-methylphenyl)-N-methoxypropionamide

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