1-Pyrrolidinecarboxylic acid, 2-[(3-amino-1-azetidinyl)carbonyl]-4-[[(4-methoxyphenyl)methyl]thio]-, (4-nitrophenyl)methyl ester, (2S,4S)-

Base Information

Chemical Name:1-Pyrrolidinecarboxylic acid, 2-[(3-amino-1-azetidinyl)carbonyl]-4-[[(4-methoxyphenyl)methyl]thio]-, (4-nitrophenyl)methyl ester, (2S,4S)-
CAS No.:153836-26-1
Molecular Formula:C24H28N4O6S
Molecular Weight:500.576
Hs Code.:
Mol file:153836-26-1.mol

1-Pyrrolidinecarboxylic acid,
2-[(3-amino-1-azetidinyl)carbonyl]-4-[[(4-methoxyphenyl)methyl]thio]-,
(4-nitrophenyl)methyl ester, (2S,4S)-

Synonyms:

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Chemical Property of 1-Pyrrolidinecarboxylic acid, 2-[(3-amino-1-azetidinyl)carbonyl]-4-[[(4-methoxyphenyl)methyl]thio]-, (4-nitrophenyl)methyl ester, (2S,4S)-

Chemical Property:

Purity/Quality:

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Technology Process of 1-Pyrrolidinecarboxylic acid, 2-[(3-amino-1-azetidinyl)carbonyl]-4-[[(4-methoxyphenyl)methyl]thio]-, (4-nitrophenyl)methyl ester, (2S,4S)-

There total 3 articles about 1-Pyrrolidinecarboxylic acid, 2-[(3-amino-1-azetidinyl)carbonyl]-4-[[(4-methoxyphenyl)methyl]thio]-, (4-nitrophenyl)methyl ester, (2S,4S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: '-carbonyldiimidazole

: 102065-89-4
azetidin-3-amine dihydrogen chloride

: 147082-06-2
(2S,4S)-4-(4-methoxybenzylthio)-1-(4-nitrobenzyloxycarbonyl)-2-pyrrolidinecarboxylic acid

: 153836-26-1
(2S,4S)-2-(3-aminoazetidin-1-ylcarbonyl)-4-(4-methoxybenzylthio)-1-(4-nitrobenzyloxycarbonyl)pyrrolidine

Guidance literature:: With sodium chloride; N-ethyl-N,N-diisopropylamine; In methanol; acetonitrile;

Reference yield:

: 102065-89-4
azetidin-3-amine dihydrogen chloride

: 147082-06-2
(2S,4S)-4-(4-methoxybenzylthio)-1-(4-nitrobenzyloxycarbonyl)-2-pyrrolidinecarboxylic acid

: 153836-26-1
(2S,4S)-2-(3-aminoazetidin-1-ylcarbonyl)-4-(4-methoxybenzylthio)-1-(4-nitrobenzyloxycarbonyl)pyrrolidine

Guidance literature:: (2S,4S)-4-(4-methoxybenzylthio)-1-(4-nitrobenzyloxycarbonyl)-2-pyrrolidinecarboxylic acid; With 1,1'-carbonyldiimidazole; In acetonitrile; at 40 ℃; for 1h;

azetidin-3-amine dihydrogen chloride; With N-ethyl-N,N-diisopropylamine; In methanol; acetonitrile; at 20 ℃; for 1h;
DOI:10.7164/antibiotics.54.1080