1H-Pyrrole-3-carboxylic acid, 1-[[(1,1-dimethylethoxy)carbonyl]amino]-2,5-dimethyl-4-[2-(phenylmethyl )benzoyl]-, methyl ester

Base Information

Chemical Name:1H-Pyrrole-3-carboxylic acid, 1-[[(1,1-dimethylethoxy)carbonyl]amino]-2,5-dimethyl-4-[2-(phenylmethyl )benzoyl]-, methyl ester
CAS No.:154708-57-3
Molecular Formula:C27H30N2O5
Molecular Weight:462.546
Hs Code.:
Mol file:154708-57-3.mol

Synonyms:

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Chemical Property of 1H-Pyrrole-3-carboxylic acid, 1-[[(1,1-dimethylethoxy)carbonyl]amino]-2,5-dimethyl-4-[2-(phenylmethyl )benzoyl]-, methyl ester

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Technology Process of 1H-Pyrrole-3-carboxylic acid, 1-[[(1,1-dimethylethoxy)carbonyl]amino]-2,5-dimethyl-4-[2-(phenylmethyl )benzoyl]-, methyl ester

There total 6 articles about 1H-Pyrrole-3-carboxylic acid, 1-[[(1,1-dimethylethoxy)carbonyl]amino]-2,5-dimethyl-4-[2-(phenylmethyl )benzoyl]-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 950203-40-4
methyl 3-tert-butoxycarbonylazo-2-butenoate

: 120935-81-1
1-<2-(phenylmethyl)benzoyl>-1,3-butanedione

: 154708-57-3
methyl 1-tert-butoxycarbonylamino-2,5-dimethyl-4-<2-(phenylmethyl)benzoyl>-1H-pyrrole-3-carboxylate

Guidance literature:: In tert-butyl alcohol; for 15h; Heating;
DOI:10.1055/s-1994-25440

Reference yield:

: 4755-81-1,935731-92-3
methyl 2-chloroacetoacetate

: 154708-57-3
methyl 1-tert-butoxycarbonylamino-2,5-dimethyl-4-<2-(phenylmethyl)benzoyl>-1H-pyrrole-3-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / diethyl ether / 3 h

2: 0.42 g / sat. aq NaHCO₃ / diethyl ether / 2.5 h

3: 72 percent / 2-methyl-propan-2-ol / 15 h / Heating

With sodium hydrogencarbonate; In diethyl ether; tert-butyl alcohol;
DOI:10.1055/s-1994-25440

Reference yield:

: 870-46-2
t-butoxycarbonylhydrazine

: 154708-57-3
methyl 1-tert-butoxycarbonylamino-2,5-dimethyl-4-<2-(phenylmethyl)benzoyl>-1H-pyrrole-3-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / diethyl ether / 3 h

2: 0.42 g / sat. aq NaHCO₃ / diethyl ether / 2.5 h

3: 72 percent / 2-methyl-propan-2-ol / 15 h / Heating

With sodium hydrogencarbonate; In diethyl ether; tert-butyl alcohol;
DOI:10.1055/s-1994-25440