2H-1,4-Oxazin-2-one, 5-chloro-6-methyl-3-phenyl-

Base Information

Chemical Name:2H-1,4-Oxazin-2-one, 5-chloro-6-methyl-3-phenyl-
CAS No.:155959-02-7
Molecular Formula:C11H8ClNO2
Molecular Weight:221.643
Hs Code.:
DSSTox Substance ID:DTXSID00464749
Nikkaji Number:J1.321.983D
Wikidata:Q82290212
Mol file:155959-02-7.mol

Synonyms:155959-02-7;2H-1,4-Oxazin-2-one, 5-chloro-6-methyl-3-phenyl-;SCHEMBL4716375;DTXSID00464749

Suppliers and Price of 2H-1,4-Oxazin-2-one, 5-chloro-6-methyl-3-phenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 2H-1,4-Oxazin-2-one, 5-chloro-6-methyl-3-phenyl-

Chemical Property:

XLogP3:2.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:221.0243562
Heavy Atom Count:15
Complexity:341

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=C(N=C(C(=O)O1)C2=CC=CC=C2)Cl

Technology Process of 2H-1,4-Oxazin-2-one, 5-chloro-6-methyl-3-phenyl-

There total 3 articles about 2H-1,4-Oxazin-2-one, 5-chloro-6-methyl-3-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 125849-94-7
3,5-dichloro-6-methyl-2(H)-1,4-oxazin-2-one

: 71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1
benzene

: 155959-02-7
5-chloro-6-methyl-3-phenyl-2(H)-1,4-oxazin-2-one

Guidance literature:: With aluminium trichloride; In dichloromethane; for 2h; Ambient temperature;
DOI:10.1016/S0040-4020(01)90431-4

Reference yield: 85.0%

: 595-90-4
tetraphenyltin(IV)

: 125849-94-7
3,5-dichloro-6-methyl-2(H)-1,4-oxazin-2-one

: 155959-02-7
5-chloro-6-methyl-3-phenyl-2(H)-1,4-oxazin-2-one

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; Heating;
DOI:10.1016/S0040-4020(00)00193-9

Reference yield: 61.0%

: 934-56-5
trimethyl(phenyl)stannane

: 125849-94-7
3,5-dichloro-6-methyl-2(H)-1,4-oxazin-2-one

: 155959-02-7
5-chloro-6-methyl-3-phenyl-2(H)-1,4-oxazin-2-one

Guidance literature:: tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; for 24h; Heating;
DOI:10.1016/j.tetlet.2004.03.183 DOI:10.1021/jo051646i