N-(2,6-Dimethylheptan-4-yl)-P,P-diphenylphosphinic amide

Base Information

Chemical Name:N-(2,6-Dimethylheptan-4-yl)-P,P-diphenylphosphinic amide
CAS No.:156301-30-3
Molecular Formula:C21H30NOP
Molecular Weight:343.449
Hs Code.:
DSSTox Substance ID:DTXSID70565691
Wikidata:Q82450917
Mol file:156301-30-3.mol

Synonyms:156301-30-3;DTXSID70565691;N-(2,6-Dimethylheptan-4-yl)-P,P-diphenylphosphinic amide

Suppliers and Price of N-(2,6-Dimethylheptan-4-yl)-P,P-diphenylphosphinic amide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(2,6-Dimethylheptan-4-yl)-P,P-diphenylphosphinic amide

Chemical Property:

XLogP3:5.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:8
Exact Mass:343.206501578
Heavy Atom Count:24
Complexity:363

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)CC(CC(C)C)NP(=O)(C1=CC=CC=C1)C2=CC=CC=C2

Technology Process of N-(2,6-Dimethylheptan-4-yl)-P,P-diphenylphosphinic amide

There total 5 articles about N-(2,6-Dimethylheptan-4-yl)-P,P-diphenylphosphinic amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 920-39-8
isopropylmagnesium bromide

: 156301-22-3
(S)-1-(Diphenyl-phosphinoyl)-2-isobutyl-aziridine

: 156301-30-3
2,6-dimethyl-4-[(diphenylphosphoryl)amino]heptane

Guidance literature:: With copper(I) bromide*diethyl sulfide; In tetrahydrofuran; -40 degC -> r.t., 10 min, reflux;
DOI:10.1016/S0040-4039(00)77020-1

Reference yield: 78.0%

: 1068-55-9
isopropylmagnesium chloride

: 174782-16-2
N,O-bis(diphenylphosphoryl)-2-(hydroxymethyl)aziridine

: 156301-30-3
2,6-dimethyl-4-[(diphenylphosphoryl)amino]heptane

Guidance literature:: With copper(I) bromide dimethylsulfide complex; In tetrahydrofuran; for 0.5h; Heating;
DOI:10.1016/S0040-4020(03)00551-9

Reference yield:

: 1499-21-4
Diphenylphosphinic chloride

: 156301-30-3
2,6-dimethyl-4-[(diphenylphosphoryl)amino]heptane

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / tetrahydrofuran / 20 h / 0 - 20 °C

1.2: 60 percent / NaH / tetrahydrofuran / 72 h / 20 °C

2.1: 78 percent / CuBr*SMe₂ / tetrahydrofuran / 0.5 h / Heating

With copper(I) bromide dimethylsulfide complex; triethylamine; In tetrahydrofuran;
DOI:10.1016/S0040-4020(03)00551-9