Pyridine, 1,2,3,6-tetrahydro-1-methyl-4-(4-methylphenyl)-

Base Information

Chemical Name:Pyridine, 1,2,3,6-tetrahydro-1-methyl-4-(4-methylphenyl)-
CAS No.:69675-08-7
Molecular Formula:C13H17N
Molecular Weight:187.285
Hs Code.:
DSSTox Substance ID:DTXSID50219968
Nikkaji Number:J438.798H
Wikidata:Q83097027
ChEMBL ID:CHEMBL99321

Synonyms:Pyridine, 1,2,3,6-tetrahydro-1-methyl-4-(4-methylphenyl)-;69675-08-7;CHEMBL99321;SCHEMBL7369176;DTXSID50219968

Suppliers and Price of Pyridine, 1,2,3,6-tetrahydro-1-methyl-4-(4-methylphenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Pyridine, 1,2,3,6-tetrahydro-1-methyl-4-(4-methylphenyl)-

Chemical Property:

Vapor Pressure:0.00256mmHg at 25°C
Boiling Point:287°Cat760mmHg
Flash Point:116.3°C
Density:0.989g/cm³
XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:187.136099547
Heavy Atom Count:14
Complexity:211

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)C2=CCN(CC2)C

Technology Process of Pyridine, 1,2,3,6-tetrahydro-1-methyl-4-(4-methylphenyl)-

There total 7 articles about Pyridine, 1,2,3,6-tetrahydro-1-methyl-4-(4-methylphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 454482-11-2
1-methyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl )-1,2,3,6-tetrahydropyridine

: 5-(p-tolyl)-5H-thianthren-5-ium trifluoromethanesulfonate

: 69675-08-7
1-methyl-4-(4-methylphenyl)-1,2,3,6-tetrahydropyridine

Guidance literature:: With bis(tri-t-butylphosphine)palladium⁽⁰⁾; sodium hydrogencarbonate; In dichloromethane; N,N-dimethyl-formamide; at 50 ℃; for 12h; Inert atmosphere; Schlenk technique;
DOI:10.1039/d0cc00641f

Reference yield:

: 1445-73-4
1-Methyl-4-piperidone

: 69675-08-7
1-methyl-4-(4-methylphenyl)-1,2,3,6-tetrahydropyridine

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / -78 °C

2: HCl, acetic acid / Heating

With hydrogenchloride; acetic acid; In tetrahydrofuran;
DOI:10.1021/jm9603882

Reference yield:

: 2417-95-0
p-tolyllithium

: 69675-08-7
1-methyl-4-(4-methylphenyl)-1,2,3,6-tetrahydropyridine

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / -78 °C

2: HCl, acetic acid / Heating

With hydrogenchloride; acetic acid; In tetrahydrofuran;
DOI:10.1021/jm9603882