Carbamodithioic acid, (4-methoxyphenyl)-, monoammonium salt

Base Information

• Chemical Name: Carbamodithioic acid, (4-methoxyphenyl)-, monoammonium salt
• CAS No.: 15866-98-5
• Molecular Formula: C8H9NOS2.H3N
• Molecular Weight: 216.328

Synonyms:

Chemical Property of Carbamodithioic acid, (4-methoxyphenyl)-, monoammonium salt

Chemical Property:

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Technology Process of Carbamodithioic acid, (4-methoxyphenyl)-, monoammonium salt

There total 1 articles about Carbamodithioic acid, (4-methoxyphenyl)-, monoammonium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

carbon disulfide (75-15-0,12122-00-8) + 4-methoxy-aniline (104-94-9) → ammonium salt of N-p-anisylamino dithiocarbamic acid (15866-98-5)

Guidance literature:

With ammonium hydroxide; at 0 - 20 ℃; for 3h;

DOI:10.1080/17415993.2016.1262373

Reference yield: 97.0%

ruthenium(III) chloride trihydrate + ammonium salt of N-p-anisylamino dithiocarbamic acid (15866-98-5) → tris(N-(4-methoxyphenyl)dithiocarbamato) ruthenium(III)

Guidance literature:

With water; In ethanol; for 0.75h;

DOI:10.1080/17415993.2016.1262373

Reference yield: 90.0%

5-bromobarbituric acid (19645-78-4) + ammonium salt of N-p-anisylamino dithiocarbamic acid (15866-98-5) → 2,4,6-trioxo-hexahydropyrimidin-5-yl 4-methoxyphenylcarbamodithioate

Guidance literature:

With Amberlyst-15; In water; at 20 ℃; for 4h; Green chemistry;

DOI:10.2174/1570178612666150108002716

upstream raw materials:

carbon disulfide

4-methoxy-aniline

Downstream raw materials:

4-hydroxy-3-(4-methoxyphenyl)thiazolidine-2-thione

4-(4-methoxy-phenyl)-5-phenylimino-[1,2,4]dithiazolidine-3-thione

3-(4-methoxy-phenyl)-4-methyl-3H-thiazole-2-thione

trans-α-Phenylzimtsaeure-(4-methoxyanilid)

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