Carbamodithioic acid, (4-chlorophenyl)-

Base Information

• Chemical Name: Carbamodithioic acid, (4-chlorophenyl)-
• CAS No.: 15867-09-1
• Molecular Formula: C7H6ClNS2
• Molecular Weight: 203.716
• Mol file: 15867-09-1.mol

Synonyms:

Chemical Property of Carbamodithioic acid, (4-chlorophenyl)-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Carbamodithioic acid, (4-chlorophenyl)-

There total 2 articles about Carbamodithioic acid, (4-chlorophenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

carbon disulfide (75-15-0,12122-00-8) + 4-chloro-aniline (106-47-8) → (4-chloro-phenyl)-dithiocarbamic acid (15867-09-1)

Guidance literature:

With ammonia; In ethanol; water; at 15 - 20 ℃;

DOI:10.3184/030823410X12628833270368

Reference yield:

4-chloro-aniline (106-47-8) → (4-chloro-phenyl)-dithiocarbamic acid (15867-09-1)

Guidance literature:

With ammonia;

Reference yield: 93.0%

2-phenylazlactone (1199-01-5,53766-22-6) + D-xylose (58-86-6) + (4-chloro-phenyl)-dithiocarbamic acid (15867-09-1) → C21H19ClN2O5S2

Guidance literature:

With 1-butyl-3-methylimidazolium hydroxide; In tetrahydrofuran; at 20 ℃; for 6.5h;

DOI:10.1139/cjc-2016-0155

upstream raw materials:

4-chloro-aniline

carbon disulfide

Downstream raw materials:

4-chloro-aniline

4-(p-chlorophenyl)-3-thiosemicarbazide

4-Chlorophenyl isothiocyanate

C₉H₇ClNO₂S₂^(1-)*Na⁽¹⁺⁾

Refernces

• 1、 Seelam, Mohan,Shaik, Bajivali,Kammela, Prasada Rao. "Cobalt mediated by desulfurization toward the synthesis of isothiocyanates". supporting information. p. 1759 - 1765. Retrieved 2016/10/31.
• 2、 Yao, Jianwen,Chen, Jing,He, Zuopeng,Sun, Wei,Fang, Hao,Xu, Wenfang. "Thiourea and thioether derivatives of sorafenib: Synthesis, crystal structure, and antiproliferative activity". . p. 3959 - 3968. Retrieved 2013/07/26.