1,4,7,10-Tetraoxadispiro[4.0.4.4]tetradecane

Base Information

• Chemical Name: 1,4,7,10-Tetraoxadispiro[4.0.4.4]tetradecane
• CAS No.: 158-95-2
• Molecular Formula: C10H16O4
• Molecular Weight: 200.235
• DSSTox Substance ID: DTXSID90483964

Synonyms:158-95-2;1,4,7,10-Tetraoxadispiro[4.0.4.4]tetradecane;DTXSID90483964

Chemical Property of 1,4,7,10-Tetraoxadispiro[4.0.4.4]tetradecane

Chemical Property:

• XLogP3: 0.3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 0
• Exact Mass: 200.10485899
• Heavy Atom Count: 14
• Complexity: 192

Purity/Quality:

99.90% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1CCC2(C3(C1)OCCO3)OCCO2

Technology Process of 1,4,7,10-Tetraoxadispiro[4.0.4.4]tetradecane

There total 3 articles about 1,4,7,10-Tetraoxadispiro[4.0.4.4]tetradecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethylene glycol (107-21-1) + cyclohexane-1,2-dione (765-87-7) → cyclohexane-1,2-dione bis(ethyleneketal) (158-95-2) + 1,4-dioxaspiro[4.5]decan-6-one (4746-96-7)

Guidance literature:

With toluene-4-sulfonic acid; In toluene; for 8h; Reflux;

DOI:10.3390/molecules17066808

Reference yield:

cyclohexane-1,2-dione (765-87-7) → cyclohexane-1,2-dione bis(ethyleneketal) (158-95-2) + 1,4-dioxaspiro[4.5]decan-6-one (4746-96-7)

Guidance literature:

With toluene-4-sulfonic acid; ethylene glycol; benzene;

DOI:10.1039/jr9550000160

Reference yield:

ethylene glycol (107-21-1) + cyclohexane-1,2-dione (765-87-7) → cyclohexane-1,2-dione bis(ethyleneketal) (158-95-2) + 2,5,7,10-tetraoxa<4.4.4>propellane (35676-38-1)

Guidance literature:

With toluene-4-sulfonic acid; benzene; Entfernen des entstehenden Wassers;

DOI:10.1039/jr9550000160

upstream raw materials:

ethylene glycol

cyclohexane-1,2-dione

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