Cyclohexanecarboxylic acid, lithium salt

Base Information

• Chemical Name: Cyclohexanecarboxylic acid, lithium salt
• CAS No.: 16090-10-1
• Molecular Formula: C7H12O2.Li
• Molecular Weight: 134.104
• Mol file: 16090-10-1.mol

Synonyms:

Chemical Property of Cyclohexanecarboxylic acid, lithium salt

Chemical Property:

Purity/Quality:

99.90% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Cyclohexanecarboxylic acid, lithium salt

There total 1 articles about Cyclohexanecarboxylic acid, lithium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

Cyclohexanecarboxylic acid (98-89-5) → cyclohexanecarboxylic acid Li-salt (16090-10-1)

Guidance literature:

With lithium methanolate; In methanol; at 5 - 20 ℃; for 4.5h;

Reference yield: 92.0%

cyclohexanecarboxylic acid Li-salt (16090-10-1) → cyclohexanecarbaldehyde (2043-61-0)

Guidance literature:

With 9-borabicyclo[3.3.1]nonane dimer; In tetrahydrofuran; for 1h; Ambient temperature;

Reference yield: 86.0%

phenethylmagnesium bromide (3277-89-2) + cyclohexanecarboxylic acid Li-salt (16090-10-1) → 1-cyclohexyl-3-phenyl-1-propanone (43125-06-0)

Guidance literature:

With Grignard reagent; N,N-diphenyl-p-methoxyphenylchloromethyleniminium chloride; copper(l) iodide; In tetrahydrofuran; dichloromethane; 1) -30 deg C, 1 h, 2) 0 deg C, 1 h;

DOI:10.1016/S0040-4039(00)85572-0

upstream raw materials:

Cyclohexanecarboxylic acid

Downstream raw materials:

1-cyclohexyl-3-phenyl-1-propanone

Cyclohexyl Methylenecyclopropyl Ketone

cyclohexanecarbaldehyde

1-cyclohexyl-4-penten-1-one

Refernces

• 1、 -. "CHEMICAL COMPOUNDS". Page/Page column 83. . Retrieved 2008/06/13.