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Cyclohexanecarboxylic acid manufacture
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High purity Various Specifications Cyclohexanecarboxylic acid CAS:98-89-5
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98-89-5 Usage

Synthesis Reference(s)

The Journal of Organic Chemistry, 22, p. 1680, 1957 DOI: 10.1021/jo01363a041Tetrahedron Letters, 21, p. 4773, 1980 DOI: 10.1016/0040-4039(80)80136-5

Purification Methods

Crystallise the acid from hot H2O (solubility is 0.2% w/w at 15o), it is soluble in organic solvents. Also distil it at as high a vacuum as possible and warm the condenser as it solidifies on cooling.The acid chloride M 146.6, has b 184o/atm, d2 5 1.096, the methyl ester has b 183o/atm, and the S-benzylisothiuronium salt has m 165-166o (from EtOH). [Beilstein 9 H 7, 9 I 5, 9 II 6, 9 III15, 9 IV 16.]

Application

Cyclohexanecarboxylic acid is a precursor to the nylon-6 precursor caprolactam via its reaction with nitrosylsulfuric acid. It can also be oxidized to cyclohexene. Cyclohexanecarboxylic acid exhibits the reactions typical of carboxylic acids, including its conversion to the acid chloride cyclohexanecarbonyl chloride.

Uses

Paint and varnish driers, dry-cleaning soaps, lubricating oils, stabilizer for rubber.

Taste threshold values

Taste characteristics at 5 ppm: fruity, woody, berry-like with green dirty nuances

Definition

ChEBI: A monocarboxylic acid that consists of cyclohexane substituted by a carboxy group.

Chemical Properties

Cyclohexanecarboxylic acid has a cheese-like odor.

Description

Cyclohexanecarboxylic acid, also known as hexahydrobenzoic acid or carboxycyclohexane, belongs to the class of organic compounds known as carboxylic acids. Carboxylic acids are compounds containing a carboxylic acid group with the formula -C(=O)OH. Cyclohexanecarboxylic acid is a weakly acidic compound (based on its pKa). Cyclohexanecarboxylic acid exists in all living organisms, ranging from bacteria to humans. Cyclohexanecarboxylic acid is an acidic, cheese, and fruity tasting compound. Outside of the human body,. A monocarboxylic acid that consists of cyclohexane substituted by a carboxy group.

Chemical Properties

White crystalline solid
InChI:InChI=1/C7H12O2/c8-7(9)6-4-2-1-3-5-6/h6H,1-5H2,(H,8,9)

98-89-5 Well-known Company Product Price

Brand (Code)Product description CAS number Packaging Price Detail
TCI America (C0470)  Cyclohexanecarboxylic Acid  >98.0%(T) 98-89-5 25g 130.00CNY Detail
TCI America (C0470)  Cyclohexanecarboxylic Acid  >98.0%(T) 98-89-5 500g 525.00CNY Detail
Alfa Aesar (A14693)  Cyclohexanecarboxylic acid, 98%    98-89-5 250g 408.0CNY Detail
Alfa Aesar (A14693)  Cyclohexanecarboxylic acid, 98%    98-89-5 500g 481.0CNY Detail
Alfa Aesar (A14693)  Cyclohexanecarboxylic acid, 98%    98-89-5 1000g 892.0CNY Detail
USP (1154649)  Cyclohexanecarboxylicacid  United States Pharmacopeia (USP) Reference Standard 98-89-5 1154649-500MG 4,647.24CNY Detail

98-89-5Synthetic route

benzoic acid
65-85-0

benzoic acid

Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

Conditions
ConditionsYield
With potassium Sodium; polyethylene oxide In tetrahydrofuran at 0℃; 12 ethylene oxide units/M(+);100%
With hydrogen In water at 100℃; under 15001.5 Torr; for 2h;100%
With C33H49ClNRh; hydrogen In 2,2,2-trifluoroethanol at 20℃; under 51005.1 Torr; for 24h; Autoclave; Molecular sieve;99%
cyclohexylmethyl alcohol
100-49-2

cyclohexylmethyl alcohol

Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

Conditions
ConditionsYield
With peracetic acid; C24H29INO5 In acetic acid at 30℃; for 24h;100%
With 4-acetylamino-2,2,6,6-tetramethylpiperidine-1-oxoammonium tetrafluoroborate In water; acetonitrile at 20℃;96%
With sodium bromate; 4 In water at 60℃; for 15h;95%
methanol
67-56-1

methanol

1-pyrenylmethyl ester of cyclohexane-carboxylic acid
111077-44-2

1-pyrenylmethyl ester of cyclohexane-carboxylic acid

A

methyl 1-pyrenylmethyl ether
91385-15-8

methyl 1-pyrenylmethyl ether

B

Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

Conditions
ConditionsYield
for 0.5h; Product distribution; Irradiation;A 90%
B 100%
4-Fluorobenzoic acid
456-22-4

4-Fluorobenzoic acid

Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

Conditions
ConditionsYield
With water In aq. phosphate buffer at 25℃; for 4.5h; pH=2.7 - 3.2; Electrochemical reaction;100%
With hydrogen In water at 20℃; under 750.075 Torr; for 4h;
Pentafluorobenzoic acid
602-94-8

Pentafluorobenzoic acid

Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

Conditions
ConditionsYield
With water In aq. phosphate buffer at 25℃; for 15h; pH=2.7 - 3.2; Electrochemical reaction;100%
cyclohexanecarbaldehyde
2043-61-0

cyclohexanecarbaldehyde

Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

Conditions
ConditionsYield
With dihydrogen peroxide; 7-(trifluoromethyl)-1,10-ethyleneisoalloxazinium chloride In water; acetonitrile at 85℃; for 18h;99%
With C4H11FeMo6NO24(3-)*3C16H36N(1+); water; oxygen; sodium carbonate at 50℃; under 760.051 Torr; for 8h; Green chemistry;99%
With 4H3N*4H(1+)*CuMo6O18(OH)6(4-); water; oxygen; sodium carbonate at 50℃; under 760.051 Torr; for 12h;99%
1,2,5,6-tetrahydrobenzoic acid
4771-80-6

1,2,5,6-tetrahydrobenzoic acid

Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

Conditions
ConditionsYield
With hydrogen; 3% Pd/C In benzene at 100℃; under 6205.94 Torr;99%
With hydrogen; 3% Pd/C In hexane at 100℃; under 6205.94 Torr;99%
With hydrogen; Rhodium chloride tri(triphenylphosphine-meta-trisulfonate) In water for 18h; Ambient temperature;95%
carbon monoxide
201230-82-2

carbon monoxide

cyclohexene
110-83-8

cyclohexene

Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

Conditions
ConditionsYield
With sulfuric acid; α,α′-bis(2-pyridyl(tert-butyl)phosphino)-o-xylene; water; palladium(II) acetylacetonate; acetic acid at 20 - 100℃; under 30003 Torr; for 20h; Inert atmosphere; Autoclave;99%
With water; bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine In 1,4-dioxane at 95℃; under 15200 Torr; for 6h; Product distribution; Rate constant; other catalyst;98%
With water; bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine In 1,4-dioxane at 95℃; under 15200 Torr; for 6h;98%
carbon dioxide
124-38-9

carbon dioxide

cyclohexylmagnesium bromide
931-50-0

cyclohexylmagnesium bromide

Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

Conditions
ConditionsYield
In tetrahydrofuran at 25℃; for 1.25h; Grignard Reaction; Inert atmosphere; Schlenk technique;99%
In tetrahydrofuran at 0℃; for 3h; Inert atmosphere;99%
β-hydroxycyclohexane monocarboxylic acid
609-69-8

β-hydroxycyclohexane monocarboxylic acid

Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

Conditions
ConditionsYield
With perchloric acid; palladium 10% on activated carbon In ethanol at 40 - 45℃; for 5h; Inert atmosphere; Large scale;98.3%
cyclohexanemethyl tert-butyldimethylsilyl ether
88773-81-3

cyclohexanemethyl tert-butyldimethylsilyl ether

Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

Conditions
ConditionsYield
With potassium fluoride; jones reagent In acetone at 0℃; for 1h;98%
cyclohexanecarboxylic acid allyl ester
16491-63-7

cyclohexanecarboxylic acid allyl ester

Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

Conditions
ConditionsYield
[(cyclopentadienyl)bis(acetonitrile)(triphenylphosphine)ruthenium(II)] hexafluorophosphate In methanol at 25℃; for 17h;97%
With formic acid; triethylamine In acetonitrile at 80℃; for 3h; Inert atmosphere;90%
With tetraethylammonium tosylate; tetrakis(triphenylphosphine) palladium(0) In acetonitrile Electrochemical reaction, Pb cathode, Pt anode;83%
[RuCp(η3-C3H5)(QA)]PF6, QA=quinaldic acid In methanol at 30℃; for 9h;99 % Spectr.
terephthalic acid
100-21-0

terephthalic acid

A

Reaxys ID: 11371951

Reaxys ID: 11371951

B

4-methylcyclohexanecarboxylic acid
4331-54-8

4-methylcyclohexanecarboxylic acid

C

Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

Conditions
ConditionsYield
With hydrogen; 5%-palladium/activated carbon In water at 150℃; under 7500.75 - 37503.8 Torr; for 2h; Purification / work up; autoclave;A 96.2%
B 3.1%
C 0.22%
cyclohexane carboxylic-methoxyethoxymethyl ester
81355-10-4

cyclohexane carboxylic-methoxyethoxymethyl ester

Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

Conditions
ConditionsYield
With carbon tetrabromide In isopropyl alcohol for 1.5h; Heating;96%
3-methylbut-2-enyl cyclohexanecarboxylate
439099-03-3

3-methylbut-2-enyl cyclohexanecarboxylate

Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

Conditions
ConditionsYield
With trimethylsilyl trifluoromethanesulfonate In dichloromethane at 20℃;96%
triisopropylsiloxymethyl cyclohexanecarboxylate

triisopropylsiloxymethyl cyclohexanecarboxylate

Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

Conditions
ConditionsYield
With lithium hydroxide In tetrahydrofuran; water at 20℃; Inert atmosphere;96%
cyclohexene-1-carboxylic acid
636-82-8

cyclohexene-1-carboxylic acid

Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

Conditions
ConditionsYield
With phenylsilane; C12H23N2O2P In tetrahydrofuran at 23℃; for 6h;94%
With diethyl ether; acetic acid; platinum Hydrogenation;
With pentaerythritol tetranitrate reductase H184F mutant; NADPH In ethanol at 25℃; for 0.0333333h; pH=7; Kinetics; aq. phosphate buffer; Inert atmosphere; Enzymatic reaction;
1-phenyl-1-cyclohexane
827-52-1

1-phenyl-1-cyclohexane

Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

Conditions
ConditionsYield
With sodium periodate; ruthenium trichloride In tetrachloromethane; water; acetonitrile for 24h; Ambient temperature;94%
S-tert-butyl cyclohexanecarbothioate
54829-37-7

S-tert-butyl cyclohexanecarbothioate

Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

Conditions
ConditionsYield
With tetrabutylammomium bromide In water; acetonitrile for 2h; Ambient temperature; electrolysis (undivided cell with platinum electrodes, 0.1 A constant current), other electrolytes, 1- and 2-propanol;94%
With tetrabutylammomium bromide In water; acetonitrile for 2h; Product distribution; Mechanism; Ambient temperature; electrolysis (undivided cell with platinum electrodes at a constant current of 0.1 A), other elctrolytes, other solvents; reaction of other thioates (electrooxidative C-S-cleavage);94%
S-tert-butyl cyclohexanecarbothioate
54829-37-7

S-tert-butyl cyclohexanecarbothioate

A

2-methylpropane-2-sulfinic acid
29099-08-9

2-methylpropane-2-sulfinic acid

B

t-butylsulfonic acid
16794-13-1

t-butylsulfonic acid

C

Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

Conditions
ConditionsYield
With tetrabutylammomium bromide; water In acetonitrile electrolysis; further conditions: LiBr, electrolysis;A n/a
B n/a
C 94%
Cyclohexanecarboxylic acid 2-thioxo-2H-pyridin-1-yl ester
105398-69-4

Cyclohexanecarboxylic acid 2-thioxo-2H-pyridin-1-yl ester

A

2-(cyclohexylsulfanyl)pyridine
119520-56-8

2-(cyclohexylsulfanyl)pyridine

B

Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

Conditions
ConditionsYield
With copper diacetate In pyridine at 0℃; Irradiation; Yields of byproduct given;A 94%
B n/a
With ferric nitrate In pyridine at 0℃; Product distribution; Irradiation; other metal ion; var. light sources; influence of water;A 50 % Chromat.
B 36 % Chromat.
N-methyl-N-tosylcyclohexanecarboxamide

N-methyl-N-tosylcyclohexanecarboxamide

Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

Conditions
ConditionsYield
With sodium hydroxide In water at 85℃; for 12h;94%
cyclohexylmagnesiumchloride
931-51-1

cyclohexylmagnesiumchloride

sodium methyl carbonate
6482-39-9

sodium methyl carbonate

Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

Conditions
ConditionsYield
In 2-methyltetrahydrofuran at 20℃; for 24h; Inert atmosphere;94%
tert-butyldimethylsilyl cyclohexylmethanoate

tert-butyldimethylsilyl cyclohexylmethanoate

methanol
67-56-1

methanol

Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

Conditions
ConditionsYield
Stage #1: tert-butyldimethylsilyl cyclohexylmethanoate; methanol; carbon tetrabromide at 20℃; for 0.5h; Irradiation;
Stage #2: at 20℃; for 2.5h;
93%
methanol
67-56-1

methanol

cyclohexanecarbaldehyde
2043-61-0

cyclohexanecarbaldehyde

A

methyl cyclohexylcarboxylate
4630-82-4

methyl cyclohexylcarboxylate

B

Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

Conditions
ConditionsYield
With dihydrogen peroxide; methyltrioxorhenium(VII); acetic acid; sodium bromide for 10h; Ambient temperature;A 92%
B n/a
cyclohexanecarbaldehyde
2043-61-0

cyclohexanecarbaldehyde

A

methyl cyclohexylcarboxylate
4630-82-4

methyl cyclohexylcarboxylate

B

Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

Conditions
ConditionsYield
With dihydrogen peroxide; methyltrioxorhenium(VII); acetic acid; sodium bromide In methanol for 10h; Ambient temperature;A 92%
B n/a
methyl cyclohexylcarboxylate
4630-82-4

methyl cyclohexylcarboxylate

Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

Conditions
ConditionsYield
With pyrographite; sodium hydroxide In water at 20℃; for 24h; Reagent/catalyst; Temperature;91%
cyclohexane carbonitrile
766-05-2

cyclohexane carbonitrile

Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

Conditions
ConditionsYield
With water; nitrile hydratase SP361 at 30℃; for 27h; in potassium phosphate buffer (pH = 7);90%
With water In dimethyl sulfoxide at 26℃; for 24h; pH=7; aq. phosphate buffer;67 %Chromat.
With pro-nitro010; water Reagent/catalyst; Enzymatic reaction;
With water In aq. phosphate buffer at 37℃; pH=7; Green chemistry; Enzymatic reaction;
Cyclohexanecarboxylic acid (E)-4-trimethylsilanyl-but-2-enyl ester
92097-22-8

Cyclohexanecarboxylic acid (E)-4-trimethylsilanyl-but-2-enyl ester

Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

Conditions
ConditionsYield
With methanol; tetrakis(triphenylphosphine) palladium(0) In dichloromethane for 2h; Ambient temperature; other esters;90%
cyclohexylcarboxamide
1122-56-1

cyclohexylcarboxamide

A

3,4,5,6-tetrafluorophthalimide
652-11-9

3,4,5,6-tetrafluorophthalimide

B

Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

Conditions
ConditionsYield
With 4,5,6,7-tetrafluoroisobenzofuran-1,3-dione at 140℃; for 144h;A n/a
B 90%
cyclohexanol
108-93-0

cyclohexanol

Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

cyclohexyl cyclohexanecarboxylate
15840-96-7

cyclohexyl cyclohexanecarboxylate

Conditions
ConditionsYield
zirconium(IV) oxide at 210℃; for 2h; in autoclave; 5 h, reflux in liquid-phase;100%
With dmap; iodine; di-2-thienyl carbonate In acetonitrile at 20℃; for 0.5h;89%
With dmap; 2-methyl-6-nitrobenzoic anhydride; triethylamine In dichloromethane at 20℃; for 20h;87%
Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

cyclohexanecarboxylic acid anhydride
22651-87-2

cyclohexanecarboxylic acid anhydride

Conditions
ConditionsYield
With triethylamine In tetrahydrofuran at 23℃; for 24h;100%
With 2,6-dimethylpyridine; tris(2,2'-bipyridyl)ruthenium dichloride; carbon tetrabromide; N,N-dimethyl-formamide at 25 - 30℃; for 12h; Inert atmosphere; Photolysis;98%
With magnesium basic carbonate; di-tert-butyl dicarbonate at 25℃; for 6h;98%
thiophenol
108-98-5

thiophenol

Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

S-phenyl cyclohexanecarbothioate
58587-03-4

S-phenyl cyclohexanecarbothioate

Conditions
ConditionsYield
With pyridine; O-phenyl phosphorodichloridate In 1,2-dimethoxyethane for 16h; Ambient temperature;100%
With tetrakis(2-methylimidazol-1-yl)silane In dichloromethane at 20℃; for 6h;98%
With dmap; methanesulfonic acid; triethylamine 1.) THF, 1 h, 2.) 0 deg C;83%
pyridine-4-carbonitrile
100-48-1

pyridine-4-carbonitrile

Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

2,6-dicyclohexylisonicotinonitrile
83001-42-7

2,6-dicyclohexylisonicotinonitrile

Conditions
ConditionsYield
With ammonium persulfate; sulfuric acid; silver nitrate In water at 50℃; for 2h;100%
With bis-[(trifluoroacetoxy)iodo]benzene In acetonitrile at 20℃; for 12h; Inert atmosphere; Irradiation; Schlenk technique;74%
2,3-diethynylquinoxaline
91-19-0

2,3-diethynylquinoxaline

Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

2-(tert-butyl)-quinoxaline
18503-48-5

2-(tert-butyl)-quinoxaline

Conditions
ConditionsYield
With ammonium persulfate; trifluoroacetic acid; silver nitrate In water; chlorobenzene for 2h; Heating;100%
1-phenyl-3-butanol
2344-70-9

1-phenyl-3-butanol

Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

1-methyl-3-phenylpropyl cyclohexanecarboxylate

1-methyl-3-phenylpropyl cyclohexanecarboxylate

Conditions
ConditionsYield
With dmap; 2-methyl-6-nitrobenzoic anhydride; triethylamine In dichloromethane at 20℃; for 20h;100%
With chloro-trimethyl-silane; 4-(trifluoromethyl)benzoic anhydride; titanium tetrachloride; silver nitrate In dichloromethane for 3h; Ambient temperature;95%
With chloro-trimethyl-silane; silver perchlorate; titanium tetrachloride; 4-(trifluoromethyl)benzoic anhydride In dichloromethane; toluene at 20℃; for 3h;95%
2-Debenzoyl-7,13-bis(triethylsilyl)baccatin III
150542-00-0

2-Debenzoyl-7,13-bis(triethylsilyl)baccatin III

Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

C43H72O11Si2
152448-67-4

C43H72O11Si2

Conditions
ConditionsYield
With dmap; dicyclohexyl-carbodiimide Ambient temperature;100%
2,3-dihydro-2H-furan
1191-99-7

2,3-dihydro-2H-furan

Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

2-tetrahydrofuranyl cyclohexanecarboxylate

2-tetrahydrofuranyl cyclohexanecarboxylate

Conditions
ConditionsYield
With methanesulfonic acid In dichloromethane at -25℃; for 2h; Esterification;100%
3,4-dihydro-2H-pyran
110-87-2

3,4-dihydro-2H-pyran

Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

2-tetrahydropyranyl cyclohexanecarboxylate

2-tetrahydropyranyl cyclohexanecarboxylate

Conditions
ConditionsYield
With methanesulfonic acid In dichloromethane at -25℃; for 4h; Esterification;100%
dimethyl sulfoxide
67-68-5

dimethyl sulfoxide

Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

(methylthio)methyl cyclohexanecarboxylate
16437-72-2

(methylthio)methyl cyclohexanecarboxylate

Conditions
ConditionsYield
With t-butyl bromide; sodium hydrogencarbonate at 35 - 45℃; for 13h; Esterification;100%
With oxalyl dichloride; triethylamine In dichloromethane at -60 - 20℃; for 0.5h; Swern oxidation;97%
With triethylamine at 160℃; for 20h; Schlenk technique; Inert atmosphere;70%
With triethylamine at 160℃; under 760.051 Torr; for 20h; Pummerer Sulfoxide Rearrangement; Schlenk technique; Inert atmosphere; Green chemistry;70%
N,O-dimethylhydroxylamine*hydrochloride
6638-79-5

N,O-dimethylhydroxylamine*hydrochloride

Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

N-methoxy-N-methylcyclohexanecarboxamide
80783-98-8

N-methoxy-N-methylcyclohexanecarboxamide

Conditions
ConditionsYield
Stage #1: Cyclohexanecarboxylic acid With 1,1'-carbonyldiimidazole In dichloromethane at 20℃; for 1h;
Stage #2: N,O-dimethylhydroxylamine*hydrochloride In dichloromethane at 20℃; for 16h;
100%
Stage #1: Cyclohexanecarboxylic acid With triethylamine; trichloromethyl chloroformate In dichloromethane at 0℃;
Stage #2: N,O-dimethylhydroxylamine*hydrochloride In dichloromethane at 25℃; for 1h;
96%
Stage #1: N,O-dimethylhydroxylamine*hydrochloride; Cyclohexanecarboxylic acid In dichloromethane at 18℃; for 0.25h;
Stage #2: With tributylphosphine; (2-pyridine-N-oxide)disulfide In dichloromethane
94%
1-phenyl-3-butanol
2344-70-9

1-phenyl-3-butanol

2-methyl-6-nitrobenzoic anhydride
434935-69-0

2-methyl-6-nitrobenzoic anhydride

Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

A

1-methyl-3-phenylpropyl cyclohexanecarboxylate

1-methyl-3-phenylpropyl cyclohexanecarboxylate

B

2-methyl-6-nitro-benzoic acid 1-methyl-3-phenyl-propyl ester

2-methyl-6-nitro-benzoic acid 1-methyl-3-phenyl-propyl ester

Conditions
ConditionsYield
With dmap; ethyl azide In dichloromethane at 20℃;A 100%
B n/a
[3-(tert-butyl-dimethyl-silanyloxy)-cyclopent-1-enyl]-methanol
461406-44-0

[3-(tert-butyl-dimethyl-silanyloxy)-cyclopent-1-enyl]-methanol

Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

cyclohexanecarboxylic acid 3-(tert-butyl-dimethyl-silanyloxy)-cyclopent-1-enylmethyl ester
461406-29-1

cyclohexanecarboxylic acid 3-(tert-butyl-dimethyl-silanyloxy)-cyclopent-1-enylmethyl ester

Conditions
ConditionsYield
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 23℃; for 1.5h;100%
Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

cyclohexanecarboxylic acid Li-salt
16090-10-1

cyclohexanecarboxylic acid Li-salt

Conditions
ConditionsYield
With lithium methanolate In methanol at 5 - 20℃; for 4.5h;100%
With n-butyllithium
1-hydroxy-2-acetonaphthone
711-79-5

1-hydroxy-2-acetonaphthone

Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

2-acetylnaphthalen-1-yl cyclohexanecarboxylate

2-acetylnaphthalen-1-yl cyclohexanecarboxylate

Conditions
ConditionsYield
Stage #1: Cyclohexanecarboxylic acid With thionyl chloride; N,N-dimethyl-formamide In dichloromethane at 40℃; for 0.666667h;
Stage #2: 1-hydroxy-2-acetonaphthone With pyridine In dichloromethane at 60℃; for 1h;
100%
With pyridine
1,3-diphenylpropan-2-ol
5381-92-0

1,3-diphenylpropan-2-ol

Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

1,3-diphenylpropan-2-yl cyclohexanecarboxylate

1,3-diphenylpropan-2-yl cyclohexanecarboxylate

Conditions
ConditionsYield
With 1-(4,6-dimethoxy-1,3,5-triazin-2-yl)-3,5-dimethylpyridin-1-ium chloride; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 24h; Reagent/catalyst;100%
Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

cyclohexanylcarbonyl chloride
2719-27-9

cyclohexanylcarbonyl chloride

Conditions
ConditionsYield
With thionyl chloride In dodecane; benzene at 20℃; for 1h; Heating / reflux;99%
With thionyl chloride In dodecane; hexane; benzene at 20℃; for 1h; Heating / reflux;99%
With phosphorus trichloride In dodecane; benzene at 20℃; for 1h; Heating / reflux;99%
methanol
67-56-1

methanol

Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

methyl cyclohexylcarboxylate
4630-82-4

methyl cyclohexylcarboxylate

Conditions
ConditionsYield
With sulfuric acid for 2.5h; Reflux;99%
With aluminum oxide; methanesulfonic acid at 80℃; for 0.116667h;98%
With sulfuric acid In dichloromethane for 15h; Heating;94%
Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

cyclohexylmethyl alcohol
100-49-2

cyclohexylmethyl alcohol

Conditions
ConditionsYield
With samarium diiodide; hexanal; samarium(III) trifluoromethanesulfonate In tetrahydrofuran; methanol; potassium hydroxide at 20℃; for 0.075h; Reduction;99%
With sodium tetrahydroborate; titanium tetrachloride In 1,2-dimethoxyethane for 14h; Ambient temperature;94%
With hydrogen; Rh/Al2O3; molybdenum hexacarbonyl In 1,2-dimethoxyethane at 150℃; under 76000 Torr; for 16h;93%
benzylamine
100-46-9

benzylamine

Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

N-benzylcyclohexanecarboxamide
35665-26-0

N-benzylcyclohexanecarboxamide

Conditions
ConditionsYield
With Bromotrichloromethane; 4-(diphenylphosphino)-benzyltrimethylammonium bromide; triethylamine In tetrahydrofuran; dichloromethane at 60℃; for 6h; Inert atmosphere;99%
With borane-ammonia complex In 5,5-dimethyl-1,3-cyclohexadiene for 6h; Reflux;99%
With 3,4,5-trifluorophenylboronic acid In xylene for 18h; Heating;96%
benzyl alcohol
100-51-6

benzyl alcohol

Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

benzyl cyclohexanecarboxylate
22733-94-4

benzyl cyclohexanecarboxylate

Conditions
ConditionsYield
With N-polystyrenylbutylpyridinium triflylimide; zirconium(IV) tetraisopropoxide; Iron(III) isopropoxide In n-heptane for 24h; Heating;99%
tetrachlorobis(tetrahydrofuran)hafnium(IV) In toluene for 7h; Heating;96%
With molecualar sevies 4A; tetrachlorobis(tetrahydrofuran)hafnium(IV) In toluene at 120℃; for 7h;96%
cycl-isopropylidene malonate
2033-24-1

cycl-isopropylidene malonate

Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

5-(((1-cyclohexyl)hydroxy)methylene)-2,2-dimethyl-1,3-dioxane-4,6-dione
132415-06-6

5-(((1-cyclohexyl)hydroxy)methylene)-2,2-dimethyl-1,3-dioxane-4,6-dione

Conditions
ConditionsYield
With diethyl cyanophosphonate; triethylamine In N,N-dimethyl-formamide at 0 - 20℃; Acylation;99%

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