Benzo(c)phenanthrene-3,4-diol, 3,4-dihydro-, trans-(+-)-

Base Information

Chemical Name:Benzo(c)phenanthrene-3,4-diol, 3,4-dihydro-, trans-(+-)-
CAS No.:73093-19-3
Molecular Formula:C₁₈H₁₄O₂
Molecular Weight:262.308
Hs Code.:
DSSTox Substance ID:DTXSID60993848
Nikkaji Number:J894.370B
Wikidata:Q82984619
Mol file:73093-19-3.mol

Synonyms:3,4-dihydroxy-3,4-dihydrobenzo(c)phenanthrene;benzo(c)phenanthrene 3,4-dihydrodiol;benzo(c)phenanthrene 3,4-dihydrodiol, (cis)-isomer

Suppliers and Price of Benzo(c)phenanthrene-3,4-diol, 3,4-dihydro-, trans-(+-)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Benzo(c)phenanthrene-3,4-diol, 3,4-dihydro-, trans-(+-)-

Chemical Property:

Vapor Pressure:7.35E-12mmHg at 25°C
Boiling Point:525.2°C at 760 mmHg
Flash Point:257.2°C
PSA：40.46000
Density:1.367g/cm³
LogP:3.41410
XLogP3:3.3
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:262.099379685
Heavy Atom Count:20
Complexity:391

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C2C(=C1)C=CC3=C2C4=C(C=C3)C(C(C=C4)O)O
Isomeric SMILES:C1=CC=C2C(=C1)C=CC3=C2C4=C(C=C3)[C@@H]([C@H](C=C4)O)O

Technology Process of Benzo(c)phenanthrene-3,4-diol, 3,4-dihydro-, trans-(+-)-

There total 3 articles about Benzo(c)phenanthrene-3,4-diol, 3,4-dihydro-, trans-(+-)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 118658-88-1
benzophenanthrene-3,4-dione

: 73093-19-3,79117-84-3,81345-49-5,86631-73-4,86631-74-5,88244-27-3
3,4-dihydroxy-3,4-dihydrobenzo[c]phenanthrene

Guidance literature:: With sodium tetrahydroborate; oxygen; In ethanol; for 126h;
DOI:10.1021/jo00265a023

Reference yield:

: 22717-95-9
3-hydroxybenzophenanthrene

: 73093-19-3,79117-84-3,81345-49-5,86631-73-4,86631-74-5,88244-27-3
3,4-dihydroxy-3,4-dihydrobenzo[c]phenanthrene

Guidance literature:: Multi-step reaction with 2 steps

1: 2.19 g / (KSO₃)2NO, Adogen 464, KH₂PO₄ / benzene / 1 h

2: 1.64 g / NaBH₄, O₂ / ethanol / 126 h

With sodium tetrahydroborate; potassium dihydrogenphosphate; adogen 464; potassium nitrososulfonate; oxygen; In ethanol; benzene;
DOI:10.1021/jo00265a023

Reference yield:

: 80285-08-1
3-hydroxybenzophenanthrene acetate

: 73093-19-3,79117-84-3,81345-49-5,86631-73-4,86631-74-5,88244-27-3
3,4-dihydroxy-3,4-dihydrobenzo[c]phenanthrene

Guidance literature:: Multi-step reaction with 3 steps

1: 2.5 g / HCl / methanol / 20 h

2: 2.19 g / (KSO₃)2NO, Adogen 464, KH₂PO₄ / benzene / 1 h

3: 1.64 g / NaBH₄, O₂ / ethanol / 126 h

With hydrogenchloride; sodium tetrahydroborate; potassium dihydrogenphosphate; adogen 464; potassium nitrososulfonate; oxygen; In methanol; ethanol; benzene;
DOI:10.1021/jo00265a023