((1R,2S,5R)-2-Isopropyl-5-methyl-cyclohexyloxy)-acetic acid (3R,4R)-3-[2-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyloxy)-acetoxy]-3,4-dihydro-benzo[c]phenanthren-4-yl ester

Base Information

• Chemical Name: ((1R,2S,5R)-2-Isopropyl-5-methyl-cyclohexyloxy)-acetic acid (3R,4R)-3-[2-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyloxy)-acetoxy]-3,4-dihydro-benzo[c]phenanthren-4-yl ester
• CAS No.: 86602-27-9
• Molecular Formula: C₄₂H₅₄O₆
• Molecular Weight: 654.887

Synonyms:

Chemical Property of ((1R,2S,5R)-2-Isopropyl-5-methyl-cyclohexyloxy)-acetic acid (3R,4R)-3-[2-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyloxy)-acetoxy]-3,4-dihydro-benzo[c]phenanthren-4-yl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of ((1R,2S,5R)-2-Isopropyl-5-methyl-cyclohexyloxy)-acetic acid (3R,4R)-3-[2-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyloxy)-acetoxy]-3,4-dihydro-benzo[c]phenanthren-4-yl ester

There total 2 articles about ((1R,2S,5R)-2-Isopropyl-5-methyl-cyclohexyloxy)-acetic acid (3R,4R)-3-[2-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyloxy)-acetoxy]-3,4-dihydro-benzo[c]phenanthren-4-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

L-menthoxyacetyl chloride (15356-62-4) + 3,4-dihydroxy-3,4-dihydrobenzo[c]phenanthrene (73093-19-3,79117-84-3,81345-49-5,86631-73-4,86631-74-5,88244-27-3) → ((1R,2S,5R)-2-Isopropyl-5-methyl-cyclohexyloxy)-acetic acid (3S,4S)-3-[2-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyloxy)-acetoxy]-3,4-dihydro-benzo[c]phenanthren-4-yl ester (86602-27-9,86631-72-3) + ((1R,2S,5R)-2-Isopropyl-5-methyl-cyclohexyloxy)-acetic acid (3R,4R)-3-[2-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyloxy)-acetoxy]-3,4-dihydro-benzo[c]phenanthren-4-yl ester (86602-27-9,86631-72-3)

Guidance literature:

In pyridine; at 4 ℃; for 12h; Yield given. Yields of byproduct given;

DOI:10.1016/S0040-4039(00)81653-6

Reference yield:

L-menthoxyacetyl chloride (15356-62-4) + 3,4-dihydroxy-3,4-dihydrobenzo[c]phenanthrene (73093-19-3,79117-84-3,81345-49-5,86631-73-4,86631-74-5,88244-27-3) → ((1R,2S,5R)-2-Isopropyl-5-methyl-cyclohexyloxy)-acetic acid (3S,4S)-3-[2-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyloxy)-acetoxy]-3,4-dihydro-benzo[c]phenanthren-4-yl ester (86602-27-9,86631-72-3) + ((1R,2S,5R)-2-Isopropyl-5-methyl-cyclohexyloxy)-acetic acid (3R,4R)-3-[2-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyloxy)-acetoxy]-3,4-dihydro-benzo[c]phenanthren-4-yl ester (86602-27-9,86631-72-3)

Guidance literature:

In pyridine; at 4 ℃; for 12h; Yield given. Yields of byproduct given;

DOI:10.1016/S0040-4039(00)81653-6

Reference yield: 100.0%

((1R,2S,5R)-2-Isopropyl-5-methyl-cyclohexyloxy)-acetic acid (3R,4R)-3-[2-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyloxy)-acetoxy]-3,4-dihydro-benzo[c]phenanthren-4-yl ester (86602-27-9,86631-72-3) → ((1R,2S,5R)-2-Isopropyl-5-methyl-cyclohexyloxy)-acetic acid (3R,4R)-3-[2-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyloxy)-acetoxy]-1,2,3,4-tetrahydro-benzo[c]phenanthren-4-yl ester (86602-28-0,86687-38-9)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethyl acetate; for 1.5h; under 760 Torr;

DOI:10.1016/S0040-4039(00)81653-6

upstream raw materials:

L-menthoxyacetyl chloride

3,4-dihydroxy-3,4-dihydrobenzo[c]phenanthrene

Downstream raw materials:

(+)-(1S,2R,3R,4S)-3,4-dihydroxy-1,2-epoxy-1,2,3,4-tetrahydrobenzo[c]phenanthrene

(+)-syn-benzo[c]phenanthrene 3,4-dihydrodiol 1,2-epoxide

((1R,2S,5R)-2-Isopropyl-5-methyl-cyclohexyloxy)-acetic acid (3R,4R)-3-[2-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyloxy)-acetoxy]-1,2,3,4-tetrahydro-benzo[c]phenanthren-4-yl ester

C₃₆H₃₄N₂O₄

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