ethyl(triphenyl)germane

Base Information

Chemical Name:ethyl(triphenyl)germane
CAS No.:2945-45-1
Molecular Formula:C20H20Ge
Molecular Weight:332.969
Hs Code.:
Mol file:2945-45-1.mol

Synonyms:

Suppliers and Price of ethyl(triphenyl)germane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 6 raw suppliers

Chemical Property of ethyl(triphenyl)germane

Chemical Property:

Vapor Pressure:3.82E-06mmHg at 25°C
Boiling Point:396.7°Cat760mmHg
Flash Point:190.8°C
Density:g/cm³

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of ethyl(triphenyl)germane

There total 14 articles about ethyl(triphenyl)germane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: Cp₂Zr(C₂H₄)(PMe₃)

: 1626-24-0
chlorotriphenylgermane

: 2945-45-1
ethyltriphenylgermane

Guidance literature:: In tetrahydrofuran; Ph3GeCl was added to the mixt in THF at room temp. and stirred for 10 min (N2); quenched with 3N aq. HCl, extd. with hexane; dried over MgSO4, concd., column chromd. on silica gel (hexane);
DOI:10.1016/S0022-328X(00)00463-0

Reference yield: 68.0%

: 594-02-5
1,1-diiodoethane

: 2816-43-5
triphenylgermane

: 2945-45-1
ethyltriphenylgermane

Guidance literature:: With Sm; In further solvent(s); to a mixt. of Sm powder and Ge compound (3:1) in THP added 3 equi. of CH2I2 at -40°C, warmed to room temp.; quenched (H2O), extd.(CH2Cl2) 3 times, dried (Na2SO4), evapd.(vac.), chromy.(silica gel);
DOI:10.1039/c1cc11256b

Reference yield: 51.0%

: 74-96-4
ethyl bromide

: CH₃(C₆H₅)((C₆H₅)3Ge)SiH

: 2945-45-1
ethyltriphenylgermane

Guidance literature:: With lithium; In tetrahydrofuran; byproducts: (MePhHSi)2; a trace amt. of Li and equiv. amt. of EtBr in ether after 12 h were added to silane, room temp., 24 h, N2 atm.; hydrolysis, extn. (ether), evapn., recrystn. (pentane);
DOI:10.1016/S0022-328X(00)98847-8