4,5-Bis{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}benzene-1,2-diamine

Base Information

• Chemical Name: 4,5-Bis{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}benzene-1,2-diamine
• CAS No.: 165254-22-8
• Molecular Formula: C20H36N2O8
• Molecular Weight: 432.514
• DSSTox Substance ID: DTXSID70572507
• Nikkaji Number: J2.590.819H
• Wikidata: Q82460870
• Mol file: 165254-22-8.mol

Synonyms:165254-22-8;4,5-Bis{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}benzene-1,2-diamine;SCHEMBL4101727;DTXSID70572507;YOTKGBDGRWVHNF-UHFFFAOYSA-N;1,2-diamino-4,5-bis[2-[2-(2-methoxyethoxy)ethoxy]ethoxy]benzene

Chemical Property of 4,5-Bis{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}benzene-1,2-diamine

Chemical Property:

• XLogP3: -1
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 10
• Rotatable Bond Count: 20
• Exact Mass: 432.24716611
• Heavy Atom Count: 30
• Complexity: 347

Purity/Quality:

99.90% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COCCOCCOCCOC1=C(C=C(C(=C1)N)N)OCCOCCOCCOC

Technology Process of 4,5-Bis{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}benzene-1,2-diamine

There total 2 articles about 4,5-Bis{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}benzene-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ortho-difluorobenzene (367-11-3) → 1,2-diamino-4,5-bis[2-[2-(2-methoxyethoxy)ethoxy]ethoxy]benzene (165254-22-8)

Guidance literature:

Multi-step reaction with 3 steps

1.1: sulfuric acid; nitric acid / 16 h / 20 - 100 °C

2.1: sodium hydride / 1,2-dimethoxyethane; mineral oil / 1 h / 20 °C / Inert atmosphere

2.2: 20 °C / Inert atmosphere

3.1: hydrogen; palladium 10% on activated carbon / methanol / 20 °C

With sulfuric acid; palladium 10% on activated carbon; hydrogen; nitric acid; sodium hydride; In methanol; 1,2-dimethoxyethane; mineral oil;

DOI:10.1021/ja308055s

Reference yield:

→ 1,2-diamino-4,5-bis[2-[2-(2-methoxyethoxy)ethoxy]ethoxy]benzene (165254-22-8)

Guidance literature:

Reference yield: 100.0%

1,2-diamino-4,5-bis[2-[2-(2-methoxyethoxy)ethoxy]ethoxy]benzene (165254-22-8) → 1,2-bis(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)-4,5-phenylenediamine dihydrochloride

Guidance literature:

With hydrogenchloride; In water; acetone;

DOI:10.1246/cl.2010.226

upstream raw materials:

ortho-difluorobenzene

Downstream raw materials:

1,2-bis[2-[2-(2-methoxyethoxy]ethoxy]ethoxy]-4,5-dinitrobenzene

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