Benzene, 1,1'-(2-diazo-1,3-propanediyl)bis-

Base Information

Chemical Name:Benzene, 1,1'-(2-diazo-1,3-propanediyl)bis-
CAS No.:166264-26-2
Molecular Formula:C15H14N2
Molecular Weight:222.29
Hs Code.:
DSSTox Substance ID:DTXSID00437539
Wikidata:Q82253055

Synonyms:Benzene, 1,1'-(2-diazo-1,3-propanediyl)bis-;166264-26-2;2-diazo 1,3-diphenyl-propane;SCHEMBL13382700;DTXSID00437539

Suppliers and Price of Benzene, 1,1'-(2-diazo-1,3-propanediyl)bis-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Benzene, 1,1'-(2-diazo-1,3-propanediyl)bis-

Chemical Property:

XLogP3:3.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:4
Exact Mass:222.115698455
Heavy Atom Count:17
Complexity:245

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)CC(=[N+]=[N-])CC2=CC=CC=C2

Technology Process of Benzene, 1,1'-(2-diazo-1,3-propanediyl)bis-

There total 3 articles about Benzene, 1,1'-(2-diazo-1,3-propanediyl)bis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 5171-98-2
Diphenylacetone hydrazone

: 166264-26-2
2-Diazo-1,3-diphenylpropane

Guidance literature:: With lead(IV) acetate; 1,1,3,3-tetramethylguanidine; In N,N-dimethyl-formamide; at -78 ℃;
DOI:10.1021/jo00120a013

Reference yield:

: 102-04-5
1,3-Diphenylpropanone

: 166264-26-2
2-Diazo-1,3-diphenylpropane

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / N₂H₄ / methanol / Heating

2: 96 percent / Pb(OAc)4, tetramethylguanidine / dimethylformamide / -78 °C

With lead(IV) acetate; 1,1,3,3-tetramethylguanidine; hydrazine; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jo00120a013