Guanosine, 2'-deoxy-3',5'-O-[1,1,3,3-tetrakis(1-methylethyl)-1,3-disiloxanediyl]-N-[3- [(trifluoroacetyl)amino]propyl]-, 6-(diphenylcarbamate)

Base Information

Chemical Name:Guanosine, 2'-deoxy-3',5'-O-[1,1,3,3-tetrakis(1-methylethyl)-1,3-disiloxanediyl]-N-[3- [(trifluoroacetyl)amino]propyl]-, 6-(diphenylcarbamate)
CAS No.:169766-18-1
Molecular Formula:C₄₀H₅₄F₃N₇O₇Si₂
Molecular Weight:858.078
Hs Code.:

Guanosine,
2'-deoxy-3',5'-O-[1,1,3,3-tetrakis(1-methylethyl)-1,3-disiloxanediyl]-N-[3-
[(trifluoroacetyl)amino]propyl]-, 6-(diphenylcarbamate)

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Chemical Property of Guanosine, 2'-deoxy-3',5'-O-[1,1,3,3-tetrakis(1-methylethyl)-1,3-disiloxanediyl]-N-[3- [(trifluoroacetyl)amino]propyl]-, 6-(diphenylcarbamate)

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Technology Process of Guanosine, 2'-deoxy-3',5'-O-[1,1,3,3-tetrakis(1-methylethyl)-1,3-disiloxanediyl]-N-[3- [(trifluoroacetyl)amino]propyl]-, 6-(diphenylcarbamate)

There total 4 articles about Guanosine, 2'-deoxy-3',5'-O-[1,1,3,3-tetrakis(1-methylethyl)-1,3-disiloxanediyl]-N-[3- [(trifluoroacetyl)amino]propyl]-, 6-(diphenylcarbamate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 69304-37-6
1,3-Dichloro-1,1,3,3-tetraisopropyldisiloxane

: 169766-18-1
Diphenyl-carbamic acid 9-((2R,3aS,9aR)-5,5,7,7-tetraisopropyl-tetrahydro-1,4,6,8-tetraoxa-5,7-disila-cyclopentacycloocten-2-yl)-2-[3-(2,2,2-trifluoro-acetylamino)-propylamino]-9H-purin-6-yl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 93 percent / Et₃N / Ambient temperature

2: 83 percent / 2-methoxy-ethanol / 100 °C

3: 81 percent / pyridine / 0 °C

4: 44 percent / Et₃N

With pyridine; triethylamine; In 2-methoxy-ethanol;
DOI:10.1016/0040-4039(96)01755-8

Reference yield:

: 154920-36-2
3',5'-O-(tetraisopropyldisiloxane-1,3-diyl)-2-chloro-2'-deoxyinosine

: 169766-18-1
Diphenyl-carbamic acid 9-((2R,3aS,9aR)-5,5,7,7-tetraisopropyl-tetrahydro-1,4,6,8-tetraoxa-5,7-disila-cyclopentacycloocten-2-yl)-2-[3-(2,2,2-trifluoro-acetylamino)-propylamino]-9H-purin-6-yl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / 2-methoxy-ethanol / 100 °C

2: 81 percent / pyridine / 0 °C

3: 44 percent / Et₃N

With pyridine; triethylamine; In 2-methoxy-ethanol;
DOI:10.1016/0040-4039(96)01755-8

Reference yield:

: 136834-39-4
2-chloro-2'-deoxyinosine

: 169766-18-1
Diphenyl-carbamic acid 9-((2R,3aS,9aR)-5,5,7,7-tetraisopropyl-tetrahydro-1,4,6,8-tetraoxa-5,7-disila-cyclopentacycloocten-2-yl)-2-[3-(2,2,2-trifluoro-acetylamino)-propylamino]-9H-purin-6-yl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 93 percent / Et₃N / Ambient temperature

2: 83 percent / 2-methoxy-ethanol / 100 °C

3: 81 percent / pyridine / 0 °C

4: 44 percent / Et₃N

With pyridine; triethylamine; In 2-methoxy-ethanol;
DOI:10.1016/0040-4039(96)01755-8