4,4'-(5'-(4-(Pyridin-4-yl)phenyl)-[1,1':3',1''-terphenyl]-4,4''-diyl)dipyridine

Base Information

Chemical Name:4,4'-(5'-(4-(Pyridin-4-yl)phenyl)-[1,1':3',1''-terphenyl]-4,4''-diyl)dipyridine
CAS No.:170165-85-2
Molecular Formula:C39H27N3
Molecular Weight:537.65200
Hs Code.:
DSSTox Substance ID:DTXSID201133092
Nikkaji Number:J1.275.022F
Mol file:170165-85-2.mol

Synonyms:170165-85-2;4,4'-(5'-(4-(Pyridin-4-yl)phenyl)-[1,1':3',1''-terphenyl]-4,4''-diyl)dipyridine;4-[4-[3,5-bis(4-pyridin-4-ylphenyl)phenyl]phenyl]pyridine;Pyridine, 4,4'-[5'-[4-(4-pyridinyl)phenyl][1,1':3',1''-terphenyl]-4,4''-diyl]bis-;YSWG505;SCHEMBL13907332;DTXSID201133092;MFCD31700775;BS-47248;Pyridine, 4,4'-[5'-[4-(4-pyridinyl)phenyl][1,1':3',1''-terphenyl]-4,4''-diyl]bis- (9CI);CS-0111315;E81379;Pyridine,4,4-[5-[4-(4-pyridinyl)phenyl][1,1:3,1-terphenyl]-4,4-diyl]bis-

Suppliers and Price of 4,4'-(5'-(4-(Pyridin-4-yl)phenyl)-[1,1':3',1''-terphenyl]-4,4''-diyl)dipyridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 8 raw suppliers

Chemical Property of 4,4'-(5'-(4-(Pyridin-4-yl)phenyl)-[1,1':3',1''-terphenyl]-4,4''-diyl)dipyridine

Chemical Property:

Boiling Point:770.3±55.0 °C(Predicted)
PKA:5.74±0.10(Predicted)
PSA：38.67000
Density:1.166±0.06 g/cm3(Predicted)
LogP:9.87360
XLogP3:8.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:6
Exact Mass:537.220497874
Heavy Atom Count:42
Complexity:655

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC(=CC=C1C2=CC=NC=C2)C3=CC(=CC(=C3)C4=CC=C(C=C4)C5=CC=NC=C5)C6=CC=C(C=C6)C7=CC=NC=C7

Technology Process of 4,4'-(5'-(4-(Pyridin-4-yl)phenyl)-[1,1':3',1''-terphenyl]-4,4''-diyl)dipyridine

There total 3 articles about 4,4'-(5'-(4-(Pyridin-4-yl)phenyl)-[1,1':3',1''-terphenyl]-4,4''-diyl)dipyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 7511-49-1
1,3,5-tris(4-bromophenyl)benzene

: 1692-15-5
4-pyridylboronic acid

: 170165-85-2
4,4'-(5'-(4-(pyridin-4-yl)phenyl)-[1,1':3',1''-terphenyl]-4,4''-diyl)dipyridine

Guidance literature:: With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; sodium carbonate; In 1,4-dioxane; water; toluene; at 110 ℃; for 96h; Inert atmosphere;
DOI:10.1002/anie.201804787

Reference yield: 79.0%

: 7511-49-1
1,3,5-tris(4-bromophenyl)benzene

: 59020-06-3
4-trimethylstannyl-pyridine

: 170165-85-2
4,4'-(5'-(4-(pyridin-4-yl)phenyl)-[1,1':3',1''-terphenyl]-4,4''-diyl)dipyridine

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; lithium chloride; In toluene; at 110 ℃;
DOI:10.1016/00404-0399(50)0983J-

Reference yield: 20.0%

: 151417-38-8
1,3,5-tris(4-iodophenyl)benzene

: 1692-15-5
4-pyridylboronic acid

: 170165-85-2
4,4'-(5'-(4-(pyridin-4-yl)phenyl)-[1,1':3',1''-terphenyl]-4,4''-diyl)dipyridine

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In tetrahydrofuran; water; for 24h; Inert atmosphere; Reflux;
DOI:10.1039/c9dt04668b