1,3,5-Tris(4-iodophenyl)benzene

Base Information

• Chemical Name: 1,3,5-Tris(4-iodophenyl)benzene
• CAS No.: 151417-38-8
• Molecular Formula: C24H15I3
• Molecular Weight: 684.097
• Hs Code.: 29039990
• European Community (EC) Number: 625-108-0
• DSSTox Substance ID: DTXSID80445591
• Nikkaji Number: J1.201.994G
• Wikidata: Q72515203
• Mol file: 151417-38-8.mol

Synonyms:151417-38-8;1,3,5-Tris(4-iodophenyl)benzene;4,4''-Diiodo-5'-(4-iodophenyl)-1,1':3',1''-terphenyl;1,1':3',1''-Terphenyl, 4,4''-diiodo-5'-(4-iodophenyl)-;1 3 5-TRIS(4-IODOPHENYL)BENZENE)90;1,3,5-tri(4-iodophenyl)benzene;C24H15I3;YSWG551;SCHEMBL1989297;DTXSID80445591;KGLWDSJGGFTHHD-UHFFFAOYSA-N;MFCD07369795;AKOS016006740;CS-W013787;AC-29169;DS-17560;1,3,5-Tris(4-iodophenyl)benzene, 98%;FT-0768643;T3084;C72875;1 3 5-TRIS(4-IODOPHENYL)BENZENE) 90;1 3 5-TRIS(4-IODOPHENYL)BENZENE) 90;A884093

Chemical Property of 1,3,5-Tris(4-iodophenyl)benzene

Chemical Property:

• Melting Point: 254-260 °C(lit.)
• Boiling Point: 600.262 °C at 760 mmHg
• Flash Point: 309.929 °C
• PSA: 0.00000
• Density: 1.946 g/cm³
• LogP: 8.50140
• Storage Temp.: Keep in dark place,Sealed in dry,Room Temperature
• XLogP3: 8.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 3
• Exact Mass: 683.8308
• Heavy Atom Count: 27
• Complexity: 364

Purity/Quality:

97% ^*data from raw suppliers

1,3,5-Tris(4-iodophenyl)benzene >98.0%(HPLC) ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 41
• Safety Statements: 26-39

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=CC=C1C2=CC(=CC(=C2)C3=CC=C(C=C3)I)C4=CC=C(C=C4)I)I
• Uses: Building block in a synthesis of C3-symmetric nano-sized polyaromatics and molecular propellers.

Technology Process of 1,3,5-Tris(4-iodophenyl)benzene

There total 6 articles about 1,3,5-Tris(4-iodophenyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

C33H42Si3 (153912-32-4) → 1,3,5-tris(4-iodophenyl)benzene (151417-38-8)

Guidance literature:

With Iodine monochloride; In dichloromethane; at 0 ℃;

DOI:10.1039/b801108g

Reference yield: 90.0%

4-Iodoacetophenone (13329-40-3) → 1,3,5-tris(4-iodophenyl)benzene (151417-38-8)

Guidance literature:

With boron tri(hydrogen sulphate); In neat liquid; at 100 ℃; for 6h; Green chemistry;

DOI:10.1080/00397911.2012.696300

Reference yield: 70.0%

→ 1,3,5-tris{N-(4-methylbiphen-4'-yl)-N-(4-methylphenyl)amino}benzene + 1,3,5-tris(4-iodophenyl)benzene (151417-38-8)

Guidance literature:

upstream raw materials:

4-Iodoacetophenone

1-ethynyl-4-iodobenzene

1,3,5-triphenylbenzene

periodic acid

Downstream raw materials:

1,3,5-tris{4-[(4-cyano)phenylethynyl]phenyl}benzene

C₅₇H₄₂O₉

C₅₁H₃₀O₉

C₅₇H₄₂O₆