Nonanoic acid, 9-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-7-hydroxy-3-[(4-methoxyphenyl) methoxy]-4,8-dimethyl-, (3R,4S,7S,8R)-

Base Information

Chemical Name:Nonanoic acid, 9-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-7-hydroxy-3-[(4-methoxyphenyl) methoxy]-4,8-dimethyl-, (3R,4S,7S,8R)-
CAS No.:170808-37-4
Molecular Formula:C35H48O6Si
Molecular Weight:592.848
Hs Code.:
Mol file:170808-37-4.mol

Synonyms:

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Chemical Property of Nonanoic acid, 9-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-7-hydroxy-3-[(4-methoxyphenyl) methoxy]-4,8-dimethyl-, (3R,4S,7S,8R)-

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Technology Process of Nonanoic acid, 9-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-7-hydroxy-3-[(4-methoxyphenyl) methoxy]-4,8-dimethyl-, (3R,4S,7S,8R)-

There total 22 articles about Nonanoic acid, 9-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-7-hydroxy-3-[(4-methoxyphenyl) methoxy]-4,8-dimethyl-, (3R,4S,7S,8R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 158497-97-3
(Z)-(3R,4S,7S,8R)-9-(tert-Butyl-diphenyl-silanyloxy)-7-hydroxy-3-(4-methoxy-benzyloxy)-4,8-dimethyl-non-5-enoic acid

: 170808-37-4
(3R,4S,7S,8R)-9-(tert-Butyl-diphenyl-silanyloxy)-7-hydroxy-3-(4-methoxy-benzyloxy)-4,8-dimethyl-nonanoic acid

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; under 760 Torr; Ambient temperature;
DOI:10.1021/ja00091a082

Reference yield:

: 91751-24-5,92817-88-4,123284-89-9,112897-04-8
(R)-3-[(tert-butyldiphenylsilyl)oxy]-2-methylpropanal

: 170808-37-4
(3R,4S,7S,8R)-9-(tert-Butyl-diphenyl-silanyloxy)-7-hydroxy-3-(4-methoxy-benzyloxy)-4,8-dimethyl-nonanoic acid

Guidance literature:: Multi-step reaction with 8 steps

1: CrCl₂, NiCl₂ / tetrahydrofuran / 4 h / Ambient temperature

2: H₂ / Pd(CaCO₃, Pb) / benzene / 760 Torr / Ambient temperature

3: DMAP, pyridine / Ambient temperature

4: PPTS / CH₂Cl₂; methanol / Ambient temperature

5: Dess-Martin periodinane / CH₂Cl₂ / Ambient temperature

6: NaClO₂ / 2-methyl-propan-2-ol; various solvent(s) / 1 h / Ambient temperature

7: 87 percent / methanolic K₂CO₃ / Ambient temperature

8: H₂ / 10percent Pd/C / ethyl acetate / 760 Torr / Ambient temperature

With pyridine; chromium dichloride; dmap; sodium chlorite; hydrogen; pyridinium p-toluenesulfonate; potassium carbonate; Dess-Martin periodane; nickel dichloride; palladium on activated charcoal; palladium on calcium fluoride poisoned with lead; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; tert-butyl alcohol; benzene;
DOI:10.1021/ja00091a082

Reference yield:

: 95514-04-8,129029-85-2,120346-83-0
(S)-3-(tert-butyldiphenylsilyloxy)-2-methylpropan-1-ol

: 170808-37-4
(3R,4S,7S,8R)-9-(tert-Butyl-diphenyl-silanyloxy)-7-hydroxy-3-(4-methoxy-benzyloxy)-4,8-dimethyl-nonanoic acid

Guidance literature:: Multi-step reaction with 9 steps

1: Dess-Martin periodinane / CH₂Cl₂ / Ambient temperature

2: CrCl₂, NiCl₂ / tetrahydrofuran / 4 h / Ambient temperature

3: H₂ / Pd(CaCO₃, Pb) / benzene / 760 Torr / Ambient temperature

4: DMAP, pyridine / Ambient temperature

5: PPTS / CH₂Cl₂; methanol / Ambient temperature

6: Dess-Martin periodinane / CH₂Cl₂ / Ambient temperature

7: NaClO₂ / 2-methyl-propan-2-ol; various solvent(s) / 1 h / Ambient temperature

8: 87 percent / methanolic K₂CO₃ / Ambient temperature

9: H₂ / 10percent Pd/C / ethyl acetate / 760 Torr / Ambient temperature

With pyridine; chromium dichloride; dmap; sodium chlorite; hydrogen; pyridinium p-toluenesulfonate; potassium carbonate; Dess-Martin periodane; nickel dichloride; palladium on activated charcoal; palladium on calcium fluoride poisoned with lead; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; tert-butyl alcohol; benzene;
DOI:10.1021/ja00091a082