Trigermane, 1,1,1,3,3,3-hexakis(1-methylethyl)-2,2-diphenyl-

Base Information

Chemical Name:Trigermane, 1,1,1,3,3,3-hexakis(1-methylethyl)-2,2-diphenyl-
CAS No.:171089-40-0
Molecular Formula:C₃₀H₅₂Ge₃
Molecular Weight:630.513
Hs Code.:
Mol file:171089-40-0.mol

Synonyms:

Suppliers and Price of Trigermane, 1,1,1,3,3,3-hexakis(1-methylethyl)-2,2-diphenyl-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Trigermane, 1,1,1,3,3,3-hexakis(1-methylethyl)-2,2-diphenyl-

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of Trigermane, 1,1,1,3,3,3-hexakis(1-methylethyl)-2,2-diphenyl-

There total 4 articles about Trigermane, 1,1,1,3,3,3-hexakis(1-methylethyl)-2,2-diphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 1031401-84-9
((CH₃)2CH)3GeN(CH₃)2

: 1675-58-7
diphenylgermane

: 171089-40-0
2,2-diphenyl-1,1,1,3,3,3-hexa-i-propyltrigermane

Guidance literature:: In acetonitrile; at 85 ℃; Schlenk technique;
DOI:10.1021/acs.organomet.6b00596

Reference yield: 30.0%

: 2816-54-8
triisopropylchlorogermane

: 1080-42-8
diphenyldibromogermane

: 171089-40-0
2,2-diphenyl-1,1,1,3,3,3-hexa-i-propyltrigermane

Guidance literature:: With samarium diiodide; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; (argon); addn. of both substrates in THF to SmI2 in HMPA/THF at room temp. over 2 h, further stirring (1 h);
DOI:10.1039/c39950002275

Reference yield:

: 2816-54-8
triisopropylchlorogermane

: 171089-40-0
2,2-diphenyl-1,1,1,3,3,3-hexa-i-propyltrigermane

Guidance literature:: Multi-step reaction with 2 steps

1: benzene / 18 h

2: acetonitrile / 85 °C / Schlenk technique

In acetonitrile; benzene;
DOI:10.1021/acs.organomet.6b00596