TRIISOPROPYLCHLOROGERMANE

Base Information

Chemical Name:TRIISOPROPYLCHLOROGERMANE
CAS No.:2816-54-8
Molecular Formula:C9H21 Cl Ge
Molecular Weight:237.309
Hs Code.:
Mol file:2816-54-8.mol

Synonyms:Germane,chlorotriisopropyl- (7CI,8CI); Chlorotriisopropylgermane; Triisopropylgermaniumchloride; Triisopropylgermyl chloride

Suppliers and Price of TRIISOPROPYLCHLOROGERMANE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 8 raw suppliers

Chemical Property of TRIISOPROPYLCHLOROGERMANE

Chemical Property:

Vapor Pressure:0.14mmHg at 25°C
Refractive Index:1.468
Boiling Point:120-2°C/30mmHg
Flash Point:60.5°C
PSA：0.00000
Density:1,092 g/cm3
LogP:4.40070

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of TRIISOPROPYLCHLOROGERMANE

There total 6 articles about TRIISOPROPYLCHLOROGERMANE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: chloro(cyclopentadienyl)(triphenylphosphine)nickel(II)

: 24004-54-4
bis(triisopropylgermyl)mercury

: {π-CpNi(PPh3)}2Hg

: 2816-54-8
triisopropylchlorogermane

: mercury

Guidance literature:: In hexane; toluene; reaction in evacuated ampul; slow addn. of (i-propyl3Ge)2Hg (in toluene) to toluenic soln. Ni-compound (20°C); left for 2 h; soln. becomes orange and pptn. of Hg; replacement of toluene by hexane;;
DOI:10.1007/BF00962028

Reference yield: 82.0%

: 7647-01-0,15364-23-5
hydrogenchloride

: C₁₁H₂₆GeO

: 2816-54-8
triisopropylchlorogermane

Guidance literature:: In diethyl ether; hexane; for 1.5h;
DOI:10.1021/acs.organomet.6b00596

Reference yield: 81.0%

: 59274-04-3
1-triisopropylgermyloxy-2-(triisopropylgermylmercurioxy)-3,5-di-tert-butylbenzene

: 100-56-1
phenylmercury(II) chloride

: 1-triisopropylgermyloxy-2-phenylmercurioxy-3,5-di-tert-butylbenzene

: 2816-54-8
triisopropylchlorogermane

: mercury

Guidance literature:: In toluene; addn. of quinone in toluene to soln. of PhHgCl (20°C), treatment(1 h); sepn. of Hg, removal of solvent (vac.), addn. of hexane, crystn. (low temp.); elem. anal.; (i-Pr)3GeCl in mother liquor not separated; GLC;
DOI:10.1007/BF00952395