9H-Carbazole, 9-benzoyl-3,6-dichloro-

Base Information

• Chemical Name: 9H-Carbazole, 9-benzoyl-3,6-dichloro-
• CAS No.: 17274-71-4
• Molecular Formula: C₁₉H₁₁Cl₂NO
• Molecular Weight: 340.208
• Mol file: 17274-71-4.mol

Synonyms:

Chemical Property of 9H-Carbazole, 9-benzoyl-3,6-dichloro-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 9H-Carbazole, 9-benzoyl-3,6-dichloro-

There total 5 articles about 9H-Carbazole, 9-benzoyl-3,6-dichloro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

9-benzoyl-9H-carbazole (19264-68-7) → 3,6-dichloro-N-benzoylcarbazole (17274-71-4) + 3-chloro-N-benzoylcarbazole

Guidance literature:

With N-chlorobenzotriazole; In chloroform; for 8h; Heating;

DOI:10.1002/jhet.5570340328

Reference yield:

N-(4-chloro-2-nitrophenyl)-N-(4-chlorophenyl)amine (24591-15-9) → 3,6-dichloro-N-benzoylcarbazole (17274-71-4)

Guidance literature:

Multi-step reaction with 4 steps

1: tin (II)-chloride; aqueous hydrochloric acid; acetic acid

2: acetic acid; NaNO₂

3: 360 °C

4: aluminium chloride; carbon disulfide

With hydrogenchloride; carbon disulfide; aluminium trichloride; acetic acid; tin(ll) chloride; sodium nitrite;

DOI:10.1039/jr9470000937

Reference yield:

4-chloro-aniline (106-47-8) → 3,6-dichloro-N-benzoylcarbazole (17274-71-4)

Guidance literature:

Multi-step reaction with 5 steps

1: potassium carbonate

2: tin (II)-chloride; aqueous hydrochloric acid; acetic acid

3: acetic acid; NaNO₂

4: 360 °C

5: aluminium chloride; carbon disulfide

With hydrogenchloride; carbon disulfide; aluminium trichloride; potassium carbonate; acetic acid; tin(ll) chloride; sodium nitrite;

DOI:10.1039/jr9470000937

upstream raw materials:

3,6-dichloro-9H-carbazole

benzoyl chloride

9-benzoyl-9H-carbazole

N-(4-chloro-2-nitrophenyl)-N-(4-chlorophenyl)amine