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Stannane, triphenyl(2-phenylethenyl)-, (Z)-

Base Information
  • Chemical Name:Stannane, triphenyl(2-phenylethenyl)-, (Z)-
  • CAS No.:17421-59-9
  • Molecular Formula:C26H22Sn
  • Molecular Weight:453.171
  • Hs Code.:
Stannane, triphenyl(2-phenylethenyl)-, (Z)-

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Chemical Property of Stannane, triphenyl(2-phenylethenyl)-, (Z)-
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Technology Process of Stannane, triphenyl(2-phenylethenyl)-, (Z)-

There total 6 articles about Stannane, triphenyl(2-phenylethenyl)-, (Z)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
triethyl borane; In hexane; toluene; addn. of Et3B in hexane to a soln. of PhCCH and Ph3SnH in toluene at 25°C under Ar, stirring for 20 min; pouring into water, extg. 3 times with ethyl acetate, washing the combined org. layers with brine, drying over Na2SO4, concg. in vac., preparative TLC on silica gel;
DOI:10.1021/ja00242a068
Guidance literature:
In tetrahydrofuran; Sonication; sonochemical irradiation of a mixt. of Ph3SnH and phenylacetylene in THF with 10 mol % AIBN under argon, 1.5h (-55 °C internal temp.);; 87 % cis selectivity;;
DOI:10.1021/ja00199a059
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