Benzene, 1,3-dibromo-2-chloro-4-methoxy-

Base Information

• Chemical Name: Benzene, 1,3-dibromo-2-chloro-4-methoxy-
• CAS No.: 174913-37-2
• Molecular Formula: C₇H₅Br₂ClO
• Molecular Weight: 300.377
• Mol file: 174913-37-2.mol

Synonyms:

Chemical Property of Benzene, 1,3-dibromo-2-chloro-4-methoxy-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzene, 1,3-dibromo-2-chloro-4-methoxy-

There total 5 articles about Benzene, 1,3-dibromo-2-chloro-4-methoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,6-dibromo-3-methoxy-aniline (808736-57-4) → 2,4-dibromo-3-chloro-anisole (174913-37-2)

Guidance literature:

With hydrogenchloride; Diazotization_.Erhitzen der Diazoniumsalz-Loesung mit Kupfer-Pulver;

Reference yield:

3-monochlorophenol (108-43-0) → 2,4-dibromo-3-chloro-anisole (174913-37-2)

Guidance literature:

Multi-step reaction with 2 steps

1: concentrated H₂SO₄ / Behandeln des mit Eis versetzten Reaktionsgemisches mit Brom und anschliessendes Kochen mit Wasser

2: aqueous NaOH

With sodium hydroxide; sulfuric acid;

DOI:10.1039/jr9300001419

Reference yield:

2,6-Dibromo-3-methoxyacetanilide (150638-00-9) → 2,4-dibromo-3-chloro-anisole (174913-37-2)

Guidance literature:

Multi-step reaction with 2 steps

1: aq.-ethanolic KOH-solution

2: aqueous HCl / Diazotization_.Erhitzen der Diazoniumsalz-Loesung mit Kupfer-Pulver

With hydrogenchloride; potassium hydroxide;

upstream raw materials:

2,6-dibromo-3-methoxy-aniline

2,4-dibromo-3-chlorophenol

dimethyl sulfate

3-monochlorophenol

Downstream raw materials:

2,4,6-tribromo-3-chloro-anisole