2,6-Dibromo-3-methoxyacetanilide

Base Information

Chemical Name:2,6-Dibromo-3-methoxyacetanilide
CAS No.:150638-00-9
Molecular Formula:C₉H₉Br₂NO₂
Molecular Weight:322.984
Hs Code.:

Synonyms:2,6-Dibromo-3-methoxyacetanilide

Suppliers and Price of 2,6-Dibromo-3-methoxyacetanilide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,6-Dibromo-3-methoxyacetanilide

Chemical Property:

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Technology Process of 2,6-Dibromo-3-methoxyacetanilide

There total 6 articles about 2,6-Dibromo-3-methoxyacetanilide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 536-90-3,918666-97-4
m-Anisidine

: 150638-00-9
2,6-Dibromo-3-methoxyacetanilide

Guidance literature:: Multi-step reaction with 4 steps

1: Br₂, gl. HOAc

2: CH₃SO₃H / Heating

3: triethylammonium formate / 5percent Pd/C / acetonitrile / 24 h / Heating

4: 10percent NaOH / methanol / Ambient temperature

With sodium hydroxide; methanesulfonic acid; bromine; triethylammonium formate; acetic acid; palladium on activated charcoal; In methanol; acetonitrile;
DOI:10.1016/S0040-4020(01)80400-2

Reference yield:

: 36255-23-9
2,4,6-tribromo-3-methoxyaniline

: 150638-00-9
2,6-Dibromo-3-methoxyacetanilide

Guidance literature:: Multi-step reaction with 3 steps

1: CH₃SO₃H / Heating

2: triethylammonium formate / 5percent Pd/C / acetonitrile / 24 h / Heating

3: 10percent NaOH / methanol / Ambient temperature

With sodium hydroxide; methanesulfonic acid; triethylammonium formate; palladium on activated charcoal; In methanol; acetonitrile;
DOI:10.1016/S0040-4020(01)80400-2

Reference yield:

: 150637-98-2
2,4,6-Tribromo-3-methoxydiacetanilide

: 150638-00-9
2,6-Dibromo-3-methoxyacetanilide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylammonium formate / 5percent Pd/C / acetonitrile / 24 h / Heating

2: 10percent NaOH / methanol / Ambient temperature

With sodium hydroxide; triethylammonium formate; palladium on activated charcoal; In methanol; acetonitrile;
DOI:10.1016/S0040-4020(01)80400-2