1,3,5-Benzenetricarboxylic acid, tris[2-[3,5-bis[5-[4-(1,1-dimethylethyl)phenyl]-1,3,4-oxadiazol-2-yl]benzo yl]hydrazide]

Base Information

• Chemical Name: 1,3,5-Benzenetricarboxylic acid, tris[2-[3,5-bis[5-[4-(1,1-dimethylethyl)phenyl]-1,3,4-oxadiazol-2-yl]benzo yl]hydrazide]
• CAS No.: 175791-97-6
• Molecular Formula: C102H96N18O12
• Molecular Weight: 1766
• Mol file: 175791-97-6.mol

Synonyms:

Chemical Property of 1,3,5-Benzenetricarboxylic acid, tris[2-[3,5-bis[5-[4-(1,1-dimethylethyl)phenyl]-1,3,4-oxadiazol-2-yl]benzo yl]hydrazide]

Chemical Property:

Purity/Quality:

99.90% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,3,5-Benzenetricarboxylic acid, tris[2-[3,5-bis[5-[4-(1,1-dimethylethyl)phenyl]-1,3,4-oxadiazol-2-yl]benzo yl]hydrazide]

There total 2 articles about 1,3,5-Benzenetricarboxylic acid, tris[2-[3,5-bis[5-[4-(1,1-dimethylethyl)phenyl]-1,3,4-oxadiazol-2-yl]benzo yl]hydrazide] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

carbon monoxide (201230-82-2) + benzene-1,3,5-tricarboxylic acid trihydrazide (36997-31-6) + 3,5-Bis[5-(4-tert-butylphenyl)-1,3,4-oxadiazol-2-yl]iodobenzene (175791-96-5) → Benzene-1,3,5-tricarboxylic acid tris(2-benzoyl>hydrazide) (175791-97-6) + 3,5-Bis-[5-(4-tert-butyl-phenyl)-[1,3,4]oxadiazol-2-yl]-benzoate2,3,4,6,7,8,9,10-octahydro-1H-pyrimido[1,2-a]azepin-5-ylium;

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; PdCL₂-PH₂P(m-C₆H₄SO₃Na); In various solvent(s); at 100 ℃; Yields of byproduct given;

Reference yield: 90.0%

carbon monoxide (201230-82-2) + 1,8-diazabicyclo[5.4.0]undec-7-ene (6674-22-2,83329-50-4) + 3,5-Bis[5-(4-tert-butylphenyl)-1,3,4-oxadiazol-2-yl]iodobenzene (175791-96-5) → Benzene-1,3,5-tricarboxylic acid tris(2-benzoyl>hydrazide) (175791-97-6) + 3,5-Bis-[5-(4-tert-butyl-phenyl)-[1,3,4]oxadiazol-2-yl]-benzoate2,3,4,6,7,8,9,10-octahydro-1H-pyrimido[1,2-a]azepin-5-ylium;

Guidance literature:

With benzene-1,3,5-tricarboxylic acid trihydrazide; PdCL₂-PH₂P(m-C₆H₄SO₃Na); In various solvent(s); at 100 ℃; Yield given;

Reference yield: 31.0%

Benzene-1,3,5-tricarboxylic acid tris(2-benzoyl>hydrazide) (175791-97-6) → 1,3,5-Trisphenyl-1,3,4-oxadiazol-5-yl>benzene

Guidance literature:

With chlorosulfonic acid; at 40 ℃; for 72h;

upstream raw materials:

carbon monoxide

benzene-1,3,5-tricarboxylic acid trihydrazide

3,5-Bis[5-(4-tert-butylphenyl)-1,3,4-oxadiazol-2-yl]iodobenzene

1,8-diazabicyclo[5.4.0]undec-7-ene