Methanone, 1,3,5-benzenetriyltris[(3,5-dibenzoylphenyl)-

Base Information

Chemical Name:Methanone, 1,3,5-benzenetriyltris[(3,5-dibenzoylphenyl)-
CAS No.:176635-99-7
Molecular Formula:C69H42O9
Molecular Weight:1015.09
Hs Code.:

Synonyms:

Suppliers and Price of Methanone, 1,3,5-benzenetriyltris[(3,5-dibenzoylphenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Methanone, 1,3,5-benzenetriyltris[(3,5-dibenzoylphenyl)-

Chemical Property:

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Methanone, 1,3,5-benzenetriyltris[(3,5-dibenzoylphenyl)-

There total 8 articles about Methanone, 1,3,5-benzenetriyltris[(3,5-dibenzoylphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 159424-15-4
1,3,5-tris(3,5-dibenzylbenzoyl)benzene

: 176635-99-7
1,3,5-tris(3,5-dibenzoylbenzoyl)benzene

Guidance literature:: With sodium dichromate;

Reference yield:

: 591-51-5
phenyllithium

: 176635-99-7
1,3,5-tris(3,5-dibenzoylbenzoyl)benzene

Guidance literature:: Multi-step reaction with 7 steps

1: tetrahydrofuran

2: LiAlH₄, AlCl₃ / diethyl ether

3: 1. ) n-BuLi / 1. ) THF, hexane, -78 deg C, 1 h, 2. ) THF, hexane, from -78 to 10 deg C,

4: 1.) n-BuLi, TMEDA / 1. ) THF, hexane, -78 deg C, 0.5 h, 2. ) THF, hexane, from -78 to 10 deg C

5: CrO₃, H₂SO₄ / acetone / 1 h / 0 - 20 °C

6: 86 percent / diethyl amine / toluene / 40 h / Heating

7: 43 percent / acetic acid, sodium dichromate dihydrate / 12 h / Heating

With chromium(VI) oxide; lithium aluminium tetrahydride; n-butyllithium; aluminium trichloride; sodium dichromate; Diethyl amine; N,N,N,N,-tetramethylethylenediamine; sulfuric acid; acetic acid; In tetrahydrofuran; diethyl ether; acetone; toluene;

Reference yield:

: 120173-41-3
5-bromobenzene-1,3-dicarbaldehyde

: 176635-99-7
1,3,5-tris(3,5-dibenzoylbenzoyl)benzene

Guidance literature:: Multi-step reaction with 7 steps

1: tetrahydrofuran

2: LiAlH₄, AlCl₃ / diethyl ether

3: 1. ) n-BuLi / 1. ) THF, hexane, -78 deg C, 1 h, 2. ) THF, hexane, from -78 to 10 deg C,

4: 1.) n-BuLi, TMEDA / 1. ) THF, hexane, -78 deg C, 0.5 h, 2. ) THF, hexane, from -78 to 10 deg C

5: CrO₃, H₂SO₄ / acetone / 1 h / 0 - 20 °C

6: 86 percent / diethyl amine / toluene / 40 h / Heating

7: 43 percent / acetic acid, sodium dichromate dihydrate / 12 h / Heating

With chromium(VI) oxide; lithium aluminium tetrahydride; n-butyllithium; aluminium trichloride; sodium dichromate; Diethyl amine; N,N,N,N,-tetramethylethylenediamine; sulfuric acid; acetic acid; In tetrahydrofuran; diethyl ether; acetone; toluene;