N,N-Dibenzylhypochlorous amide

Base Information

• Chemical Name: N,N-Dibenzylhypochlorous amide
• CAS No.: 17761-41-0
• Molecular Formula: C14H14ClN
• Molecular Weight: 231.725
• DSSTox Substance ID: DTXSID70530728
• Nikkaji Number: J2.578.556H
• Wikidata: Q82402050
• Mol file: 17761-41-0.mol

Synonyms:17761-41-0;N,N-Dibenzylhypochlorous amide;SCHEMBL7867637;DTXSID70530728

Chemical Property of N,N-Dibenzylhypochlorous amide

Chemical Property:

• XLogP3: 3.6
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 4
• Exact Mass: 231.0814771
• Heavy Atom Count: 16
• Complexity: 163

Purity/Quality:

99.90% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1=CC=C(C=C1)CN(CC2=CC=CC=C2)Cl

Technology Process of N,N-Dibenzylhypochlorous amide

There total 4 articles about N,N-Dibenzylhypochlorous amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

dibenzylamine (103-49-1) → N-chloro-N-(phenylmethyl)-benzenemethanamine (17761-41-0)

Guidance literature:

With N-chloro-succinimide; In dichloromethane; at -10 - 20 ℃; for 0.25h; Inert atmosphere;

DOI:10.1016/j.tetlet.2010.11.142

Reference yield:

→ N-chloro-N-(phenylmethyl)-benzenemethanamine (17761-41-0)

Guidance literature:

With sodium hypochlorite;

Reference yield:

acetic acid-(2,4,N-trichloro-anilide) (112160-74-4) + dibenzylamine (103-49-1) → N-chloro-N-(phenylmethyl)-benzenemethanamine (17761-41-0)

Guidance literature:

With chloroform;

upstream raw materials:

chloroform

acetic acid-(2,4,N-trichloro-anilide)

dibenzylamine

Downstream raw materials:

dibenzylnitrosamine

dibenzylammonium nitrate

benzaldehyde

4-(N,N-dibenzylamino)benzonitrile