trimethyl-[[(2S,5S)-2-methyl-3-oxo-1,3-oxathiolan-5-yl]methyl]azanium iodide

Base Information

• Chemical Name: trimethyl-[[(2S,5S)-2-methyl-3-oxo-1,3-oxathiolan-5-yl]methyl]azanium iodide
• CAS No.: 109280-12-8
• Molecular Formula: C₈H₁₈NO₂S*I
• Molecular Weight: 319.207
• Mol file: 109280-12-8.mol

Synonyms:1,3-Oxathiolane-5-methanaminium,N,N,N,2-tetramethyl-, iodide, 3-oxide, (2a,3b,5a)-(?à)-

Chemical Property of trimethyl-[[(2S,5S)-2-methyl-3-oxo-1,3-oxathiolan-5-yl]methyl]azanium iodide

Chemical Property:

• PSA: 45.51000
• LogP: -1.94420

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of trimethyl-[[(2S,5S)-2-methyl-3-oxo-1,3-oxathiolan-5-yl]methyl]azanium iodide

There total 9 articles about trimethyl-[[(2S,5S)-2-methyl-3-oxo-1,3-oxathiolan-5-yl]methyl]azanium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-methyl-5-dimethylaminomethyl-1,3-oxathiolane (58327-01-8) → (+/-)-c-2-methyl-r-5-<(dimethylamino)methyl>-1,3-oxathiolane t-3-oxide methiodide (109280-12-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 65 percent / H₂O₂ 30percent / acetic acid / 0.5 h / Ambient temperature

2: diethyl ether / Ambient temperature

With dihydrogen peroxide; In diethyl ether; acetic acid;

Reference yield:

2-methyl-5-dimethylaminomethyl-1,3-oxathiolane (58327-01-8) → Trimethyl-((2S,3R,5R)-2-methyl-3-oxo-3λ4-[1,3]oxathiolan-5-ylmethyl)-ammonium; iodide (80551-80-0,80551-81-1,80629-19-2,80629-22-7,96094-68-7,98461-18-8,109280-05-9,109280-06-0,109280-08-2,109280-12-8,109280-13-9,109361-04-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 6.5 percent / H₂O₂ 30percent / acetic acid / 0.5 h / Ambient temperature

2: diethyl ether / Ambient temperature

With dihydrogen peroxide; In diethyl ether; acetic acid;

Reference yield:

2-methyl-5-dimethylaminomethyl-1,3-oxathiolane (58327-01-8) → Trimethyl-((2S,3S,5R)-2-methyl-3-oxo-3λ4-[1,3]oxathiolan-5-ylmethyl)-ammonium; iodide (80551-80-0,80551-81-1,80629-19-2,80629-22-7,96094-68-7,98461-18-8,109280-05-9,109280-06-0,109280-08-2,109280-12-8,109280-13-9,109361-04-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 12 percent / H₂O₂ 30percent / acetic acid / 0.5 h / Ambient temperature

2: diethyl ether / Ambient temperature

With dihydrogen peroxide; In diethyl ether; acetic acid;

upstream raw materials:

(+/-)-c-2-methyl-r-5-<(dimethylamino)methyl>-1,3-oxathiolane t-3-oxide

methyl iodide

2-methyl-5-dimethylaminomethyl-1,3-oxathiolane

2c-methyl-5r-chloromethyl-1,3-oxathiolane-3t-sulfoxide

Refernces