Technology Process of Imidazolidine, 2-(3,5-diiodophenyl)-1,3-dihydroxy-4,4,5,5-tetramethyl-
There total 5 articles about Imidazolidine, 2-(3,5-diiodophenyl)-1,3-dihydroxy-4,4,5,5-tetramethyl- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
2,3-bis(hydroxyamino)-2,3-dimethylbutane monosulfate;
In
tetrahydrofuran; methanol;
for 72h;
Ambient temperature;
DOI:10.1039/jm9960601745
- Guidance literature:
-
Multi-step reaction with 3 steps
1: NBS, benzoyl peroxide / 1,2-dichloro-ethane / 6 h / Heating
2: 1.) hexamethylenetetraamine, 2.) AcOH, aq. HCl / 1.) CHCl3, reflux, 15 h, 2.) reflux, 30 min
3: 55 percent / 2,3-bis(hydroxyamino)-2,3-dimethylbutane monosulfate salt / methanol; tetrahydrofuran / 72 h / Ambient temperature
With
hydrogenchloride; N-Bromosuccinimide; Perbenzoic acid; hexamethylenetetramine; acetic acid; 2,3-bis(hydroxyamino)-2,3-dimethylbutane monosulfate;
In
tetrahydrofuran; methanol; 1,2-dichloro-ethane;
DOI:10.1039/jm9960601745
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1.) hexamethylenetetraamine, 2.) AcOH, aq. HCl / 1.) CHCl3, reflux, 15 h, 2.) reflux, 30 min
2: 55 percent / 2,3-bis(hydroxyamino)-2,3-dimethylbutane monosulfate salt / methanol; tetrahydrofuran / 72 h / Ambient temperature
With
hydrogenchloride; hexamethylenetetramine; acetic acid; 2,3-bis(hydroxyamino)-2,3-dimethylbutane monosulfate;
In
tetrahydrofuran; methanol;
DOI:10.1039/jm9960601745
