N-Benzyl-4-(benzyloxy)but-2-en-1-amine

Base Information

Chemical Name:N-Benzyl-4-(benzyloxy)but-2-en-1-amine
CAS No.:184228-84-0
Molecular Formula:C18H21NO
Molecular Weight:267.371
Hs Code.:
DSSTox Substance ID:DTXSID70707938
Mol file:184228-84-0.mol

Synonyms:184228-84-0;N-Benzyl-4-(benzyloxy)but-2-en-1-amine;DTXSID70707938

Suppliers and Price of N-Benzyl-4-(benzyloxy)but-2-en-1-amine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of N-Benzyl-4-(benzyloxy)but-2-en-1-amine

Chemical Property:

XLogP3:2.9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:8
Exact Mass:267.162314293
Heavy Atom Count:20
Complexity:252

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)CNCC=CCOCC2=CC=CC=C2

Technology Process of N-Benzyl-4-(benzyloxy)but-2-en-1-amine

There total 3 articles about N-Benzyl-4-(benzyloxy)but-2-en-1-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 925460-38-4
(Z)-N-benzyl-N-(4-(benzyloxy)but-2-enyl)-2,4-dinitro-benzenesulfonamide

: 184228-84-0
(Z)-N-benzyl-4-(benzyloxy)but-2-en-1-amine

Guidance literature:: With mercaptoacetic acid; triethylamine; In dichloromethane; at 20 ℃;
DOI:10.1021/jo062178v

Reference yield:

: 81028-03-7
(Z)-4-benzyloxy-but-2-en-1-ol

: 184228-84-0
(Z)-N-benzyl-4-(benzyloxy)but-2-en-1-amine

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / PPh₃; DIAD / tetrahydrofuran / 20 °C

2: 74 percent / Et₃N; mercaptoacetic acid / CH₂Cl₂ / 20 °C

With di-isopropyl azodicarboxylate; mercaptoacetic acid; triethylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo062178v

Reference yield:

: 57620-22-1
N-benzyl-2,4-dinitro-benzenesulfonamide

: 184228-84-0
(Z)-N-benzyl-4-(benzyloxy)but-2-en-1-amine

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / PPh₃; DIAD / tetrahydrofuran / 20 °C

2: 74 percent / Et₃N; mercaptoacetic acid / CH₂Cl₂ / 20 °C

With di-isopropyl azodicarboxylate; mercaptoacetic acid; triethylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo062178v