Technology Process of Benzene, 1-(2-nitro-1-nonenyl)-3,5-bis(phenylmethoxy)-
There total 1 articles about Benzene, 1-(2-nitro-1-nonenyl)-3,5-bis(phenylmethoxy)- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
N-butylamine;
In
toluene;
for 26h;
Heating;
DOI:10.1071/ch9960917
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) H2, 2.) sodium metabisulfite / 1.) 10percent Pd/C / 1.) acetic acid, ethyl acetate, 67 h, 2.) 60percent aqueous ethanol, reflux, 3 h
2: 20 percent / titanium(IV) chloride / CH2Cl2 / 0.25 h / -10 °C
3: sodium hydrogen carbonate / dimethylformamide / 23.5 h
With
sodium disulfite; hydrogen; titanium tetrachloride; sodium hydrogencarbonate;
palladium on activated charcoal;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1071/ch9960917
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1.) H2, 2.) sodium metabisulfite / 1.) 10percent Pd/C / 1.) acetic acid, ethyl acetate, 67 h, 2.) 60percent aqueous ethanol, reflux, 3 h
2: 20 percent / titanium(IV) chloride / CH2Cl2 / 0.25 h / -10 °C
With
sodium disulfite; hydrogen; titanium tetrachloride;
palladium on activated charcoal;
In
dichloromethane;
DOI:10.1071/ch9960917