Benzoic acid, 2-[(2-heptyl-1,3-dioxolan-2-yl)methyl]-6-hydroxy-4-(phenylmethoxy)-, 3-methoxy-5-(2-oxononyl)-4-[(phenylmethoxy)carbonyl]phenyl ester

Base Information

Chemical Name:Benzoic acid, 2-[(2-heptyl-1,3-dioxolan-2-yl)methyl]-6-hydroxy-4-(phenylmethoxy)-, 3-methoxy-5-(2-oxononyl)-4-[(phenylmethoxy)carbonyl]phenyl ester
CAS No.:184375-07-3
Molecular Formula:C49H60O10
Molecular Weight:809.009
Hs Code.:
Mol file:184375-07-3.mol

Benzoic acid,
2-[(2-heptyl-1,3-dioxolan-2-yl)methyl]-6-hydroxy-4-(phenylmethoxy)-,
3-methoxy-5-(2-oxononyl)-4-[(phenylmethoxy)carbonyl]phenyl ester

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Chemical Property of Benzoic acid, 2-[(2-heptyl-1,3-dioxolan-2-yl)methyl]-6-hydroxy-4-(phenylmethoxy)-, 3-methoxy-5-(2-oxononyl)-4-[(phenylmethoxy)carbonyl]phenyl ester

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Technology Process of Benzoic acid, 2-[(2-heptyl-1,3-dioxolan-2-yl)methyl]-6-hydroxy-4-(phenylmethoxy)-, 3-methoxy-5-(2-oxononyl)-4-[(phenylmethoxy)carbonyl]phenyl ester

There total 16 articles about Benzoic acid, 2-[(2-heptyl-1,3-dioxolan-2-yl)methyl]-6-hydroxy-4-(phenylmethoxy)-, 3-methoxy-5-(2-oxononyl)-4-[(phenylmethoxy)carbonyl]phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 184374-82-1
benzyl 4-benzyloxy-2-methoxy-6-(2'-oxononyl)benzoate

: 184374-84-3
4-benzyloxy-6-[(2'-heptyl-1',3'-dioxolan-2'-yl)methyl]-2-hydroxybenzoic acid

: 184375-07-3
benzyl 2'-O-methylnorsuperphyllinate ethylene ketal

Guidance literature:: With dicyclohexyl-carbodiimide; In toluene; Ambient temperature;
DOI:10.1071/ch9960917

Reference yield:

: 629-37-8
1-nitrooctane

: 184375-07-3
benzyl 2'-O-methylnorsuperphyllinate ethylene ketal

Guidance literature:: Multi-step reaction with 9 steps

1: 80 percent / butylamine / toluene / 26 h / Heating

2: 1.) H₂, 2.) sodium metabisulfite / 1.) 10percent Pd/C / 1.) acetic acid, ethyl acetate, 67 h, 2.) 60percent aqueous ethanol, reflux, 3 h

3: 20 percent / titanium(IV) chloride / CH₂Cl₂ / 0.25 h / -10 °C

4: sodium hydrogen carbonate / dimethylformamide / 23.5 h

5: 75 percent / sodium hydrogen carbonate / dimethylformamide / 25 h / Ambient temperature

6: 1.) sulfamic acid, 2.) sodium chlorite / 1.) dioxan, 2.) dioxan, water, r.t., 2 h

7: H₂ / 10percent Pd/C / ethyl acetate / 18 h

8: sodium hydrogen carbonate / dimethylformamide / 23.5 h / Ambient temperature

9: 67 percent / N,N-dicyclohexylcarbodiimide / toluene / Ambient temperature

With sodium chlorite; sodium disulfite; aminosulfonic acid; hydrogen; titanium tetrachloride; sodium hydrogencarbonate; N-butylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene;
DOI:10.1071/ch9960917

Reference yield:

: 14615-72-6
3,5-dibenzyloxybenzaldehyde

: 184375-07-3
benzyl 2'-O-methylnorsuperphyllinate ethylene ketal

Guidance literature:: Multi-step reaction with 9 steps

1: 80 percent / butylamine / toluene / 26 h / Heating

2: 1.) H₂, 2.) sodium metabisulfite / 1.) 10percent Pd/C / 1.) acetic acid, ethyl acetate, 67 h, 2.) 60percent aqueous ethanol, reflux, 3 h

3: 20 percent / titanium(IV) chloride / CH₂Cl₂ / 0.25 h / -10 °C

4: sodium hydrogen carbonate / dimethylformamide / 23.5 h

5: 75 percent / sodium hydrogen carbonate / dimethylformamide / 25 h / Ambient temperature

6: 1.) sulfamic acid, 2.) sodium chlorite / 1.) dioxan, 2.) dioxan, water, r.t., 2 h

7: H₂ / 10percent Pd/C / ethyl acetate / 18 h

8: sodium hydrogen carbonate / dimethylformamide / 23.5 h / Ambient temperature

9: 67 percent / N,N-dicyclohexylcarbodiimide / toluene / Ambient temperature

With sodium chlorite; sodium disulfite; aminosulfonic acid; hydrogen; titanium tetrachloride; sodium hydrogencarbonate; N-butylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene;
DOI:10.1071/ch9960917