Technology Process of Benzoic acid,
2-heptyl-4-[[2-hydroxy-6-(2-oxononyl)-4-(phenylmethoxy)benzoyl]oxy]-6-
methoxy-, phenylmethyl ester
There total 10 articles about Benzoic acid,
2-heptyl-4-[[2-hydroxy-6-(2-oxononyl)-4-(phenylmethoxy)benzoyl]oxy]-6-
methoxy-, phenylmethyl ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogenchloride;
In
methanol;
for 2h;
Ambient temperature;
DOI:10.1071/ch9960917
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 19 percent / sodium hydrogen carbonate / dimethylformamide / 21 h
2: 92 percent / sodium hydroxide / H2O; dimethylsulfoxide / 17 h / 94 °C
3: 38 percent / N,N-dicyclohexylcarbodiimide / toluene / Ambient temperature
4: 88 percent / 5M HCl / methanol / 2 h / Ambient temperature
With
hydrogenchloride; sodium hydroxide; sodium hydrogencarbonate; dicyclohexyl-carbodiimide;
In
methanol; water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;
DOI:10.1071/ch9960917
- Guidance literature:
-
Multi-step reaction with 8 steps
1: 81 percent / pyridinium dichromate / CH2Cl2 / 22 h / Heating
2: 48 percent / toluene / 21 h / 50 °C
3: 1.) sodium, ethanol / 1.) r.t., 30 min, 2.) ethanol, reflux, 24 h
5: 19 percent / sodium hydrogen carbonate / dimethylformamide / 21 h
6: 92 percent / sodium hydroxide / H2O; dimethylsulfoxide / 17 h / 94 °C
7: 38 percent / N,N-dicyclohexylcarbodiimide / toluene / Ambient temperature
8: 88 percent / 5M HCl / methanol / 2 h / Ambient temperature
With
hydrogenchloride; sodium hydroxide; dipyridinium dichromate; ethanol; sodium; sodium hydrogencarbonate; dicyclohexyl-carbodiimide;
In
methanol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;
DOI:10.1071/ch9960917