N-[(5-methoxy-3-nitro-6-oxocyclohexa-2,4-dien-1-ylidene)methyl]-5-methyl-1H-pyrazole-3-carbohydrazide

Base Information

Chemical Name:N-[(5-methoxy-3-nitro-6-oxocyclohexa-2,4-dien-1-ylidene)methyl]-5-methyl-1H-pyrazole-3-carbohydrazide
CAS No.:5871-79-4
Molecular Formula:C13H13N5O5
Molecular Weight:270.288
Hs Code.:
DSSTox Substance ID:DTXSID60700453

Synonyms:DTXSID60700453;N-[(5-methoxy-3-nitro-6-oxocyclohexa-2,4-dien-1-ylidene)methyl]-5-methyl-1H-pyrazole-3-carbohydrazide

Suppliers and Price of N-[(5-methoxy-3-nitro-6-oxocyclohexa-2,4-dien-1-ylidene)methyl]-5-methyl-1H-pyrazole-3-carbohydrazide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[(5-methoxy-3-nitro-6-oxocyclohexa-2,4-dien-1-ylidene)methyl]-5-methyl-1H-pyrazole-3-carbohydrazide

Chemical Property:

Boiling Point:491.9°Cat760mmHg
Flash Point:251.3°C
Density:1.48g/cm³
XLogP3:0.3
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:3
Exact Mass:319.09166853
Heavy Atom Count:23
Complexity:633

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=NN1)C(=O)N(C=C2C=C(C=C(C2=O)OC)[N+](=O)[O-])N

Technology Process of N-[(5-methoxy-3-nitro-6-oxocyclohexa-2,4-dien-1-ylidene)methyl]-5-methyl-1H-pyrazole-3-carbohydrazide

There total 2 articles about N-[(5-methoxy-3-nitro-6-oxocyclohexa-2,4-dien-1-ylidene)methyl]-5-methyl-1H-pyrazole-3-carbohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 83-01-2
diphenylcarbamic chloride

: 56-40-6,18875-39-3,25718-94-9
glycine

: 5871-79-4
2-(3,3-diphenylureido)acetic acid

Guidance literature:: With potassium carbonate; In water; acetone; at 70 ℃;
DOI:10.1016/j.tet.2014.10.033

Reference yield:

: 5871-79-4
2-(3,3-diphenylureido)acetic acid

Guidance literature:: N,N-Diphenyl-carbamoylchlorid, Glycin, sd. wss. A., NaHCO3;

Reference yield: 91.0%

: 5871-79-4
2-(3,3-diphenylureido)acetic acid

: 100-46-9
benzylamine

: N-benzyl-2-(3,3-diphenylureido)acetamide

Guidance literature:: 2-(3,3-diphenylureido)acetic acid; With 1,1'-carbonyldiimidazole; In ethyl acetate; at 20 ℃; for 1h;

benzylamine; In ethyl acetate; for 1h; Reflux;
DOI:10.1016/j.tet.2014.10.033