Benzoic acid, 3,5-bis(phenylmethoxy)-4-[2-(phenylmethoxy)-6-[(phenylmethoxy)carbon yl]benzoyl]-, 3-(4-hydroxyphenyl)-2-[(phenylsulfonyl)amino]propyl ester

Base Information

Chemical Name:Benzoic acid, 3,5-bis(phenylmethoxy)-4-[2-(phenylmethoxy)-6-[(phenylmethoxy)carbon yl]benzoyl]-, 3-(4-hydroxyphenyl)-2-[(phenylsulfonyl)amino]propyl ester
CAS No.:184592-48-1
Molecular Formula:C58H49NO11S
Molecular Weight:968.093
Hs Code.:
Mol file:184592-48-1.mol

Benzoic acid,
3,5-bis(phenylmethoxy)-4-[2-(phenylmethoxy)-6-[(phenylmethoxy)carbon
yl]benzoyl]-, 3-(4-hydroxyphenyl)-2-[(phenylsulfonyl)amino]propyl ester

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Chemical Property of Benzoic acid, 3,5-bis(phenylmethoxy)-4-[2-(phenylmethoxy)-6-[(phenylmethoxy)carbon yl]benzoyl]-, 3-(4-hydroxyphenyl)-2-[(phenylsulfonyl)amino]propyl ester

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Technology Process of Benzoic acid, 3,5-bis(phenylmethoxy)-4-[2-(phenylmethoxy)-6-[(phenylmethoxy)carbon yl]benzoyl]-, 3-(4-hydroxyphenyl)-2-[(phenylsulfonyl)amino]propyl ester

There total 9 articles about Benzoic acid, 3,5-bis(phenylmethoxy)-4-[2-(phenylmethoxy)-6-[(phenylmethoxy)carbon yl]benzoyl]-, 3-(4-hydroxyphenyl)-2-[(phenylsulfonyl)amino]propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 184592-47-0
(+/-)-benzyl 2-[(2,6-bis(benzyloxy)-4-{[(2-[N-(methoxymethylene)-N-(phenylsulfonyl)amino]-3-{4-[(methoxymethylene)oxy]phenyl}propyl)oxy]carbonyl}phenyl)carbonyl]-3-(benzyloxy)benzoate

: 184592-48-1
(+/-)-benzyl 2-({2,6-bis(benzyloxy)-4-[({3-(4-hydroxyphenyl)-2-[(phenylsulfonyl)amino]propyl}oxy)carbonyl]phenyl}carbonyl)-3-(benzyloxy)benzoate

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; for 24h;
DOI:10.1021/jm960581w

Reference yield:

: 184759-46-4
N-(phenylsulfonyl)-DL-tyrosine

: 184592-48-1
(+/-)-benzyl 2-({2,6-bis(benzyloxy)-4-[({3-(4-hydroxyphenyl)-2-[(phenylsulfonyl)amino]propyl}oxy)carbonyl]phenyl}carbonyl)-3-(benzyloxy)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: 46 percent / N,N-diisopropylethylamine / acetonitrile / 1.5 h / 0 °C

2: 92 percent / LiBH₄ / tetrahydrofuran / 18 h

3: DBU / tetrahydrofuran / 72 h

4: 100 percent / 0.5 N HCl / dioxane / 24 h

With hydrogenchloride; lithium borohydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; 1,4-dioxane; acetonitrile;
DOI:10.1021/jm960581w

Reference yield:

: 3417-91-2,3728-20-9,68697-61-0
tyrosine methyl ester hydrochloride

: 184592-48-1
(+/-)-benzyl 2-({2,6-bis(benzyloxy)-4-[({3-(4-hydroxyphenyl)-2-[(phenylsulfonyl)amino]propyl}oxy)carbonyl]phenyl}carbonyl)-3-(benzyloxy)benzoate

Guidance literature:: Multi-step reaction with 6 steps

1: 40 percent / 1 N NaOH / CH₂Cl₂ / 2 h

2: 100 percent / aq. KOH / ethanol / 48 h / 60 °C

3: 46 percent / N,N-diisopropylethylamine / acetonitrile / 1.5 h / 0 °C

4: 92 percent / LiBH₄ / tetrahydrofuran / 18 h

5: DBU / tetrahydrofuran / 72 h

6: 100 percent / 0.5 N HCl / dioxane / 24 h

With hydrogenchloride; potassium hydroxide; sodium hydroxide; lithium borohydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; acetonitrile;
DOI:10.1021/jm960581w