Trisilane, 1-chloro-2-(chloromethylphenylsilyl)-1,2,3,3,3-pentamethyl-1-phenyl-

Base Information

Chemical Name:Trisilane, 1-chloro-2-(chloromethylphenylsilyl)-1,2,3,3,3-pentamethyl-1-phenyl-
CAS No.:184678-45-3
Molecular Formula:C₁₈H₂₈Cl₂Si₄
Molecular Weight:427.668
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Trisilane, 1-chloro-2-(chloromethylphenylsilyl)-1,2,3,3,3-pentamethyl-1-phenyl-

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Technology Process of Trisilane, 1-chloro-2-(chloromethylphenylsilyl)-1,2,3,3,3-pentamethyl-1-phenyl-

There total 2 articles about Trisilane, 1-chloro-2-(chloromethylphenylsilyl)-1,2,3,3,3-pentamethyl-1-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 286853-73-4
C₂₆H₄₈N₂Si₄

: 184678-45-3
C₁₈H₂₈Cl₂Si₄

Guidance literature:: With hydrogenchloride; In diethyl ether; at 0 ℃; for 0.333333h;
DOI:10.1016/S0022-328X(00)00077-2

Reference yield:

: 140438-37-5
C₁₁H₁₈NSi^(1-)*Li⁽¹⁺⁾

: 184678-45-3
C₁₈H₂₈Cl₂Si₄

Guidance literature:: Multi-step reaction with 2 steps

1: 600 mg / i-PrMgBr / tetrahydrofuran; diethyl ether / 0 - 20 °C

2: 455 mg / HCl / diethyl ether / 0.33 h / 0 °C

With hydrogenchloride; isopropylmagnesium bromide; In tetrahydrofuran; diethyl ether; 1: silylation / 2: Chlorination;
DOI:10.1016/S0022-328X(00)00077-2