Furo(2,3,4-cd)isoindole-2,6-dione, octahydro-4,5-dibromo-7-((4-methoxyphenyl)methyl)-3-methyl-7a-(phenylmethyl)-

Base Information

Chemical Name:Furo(2,3,4-cd)isoindole-2,6-dione, octahydro-4,5-dibromo-7-((4-methoxyphenyl)methyl)-3-methyl-7a-(phenylmethyl)-
CAS No.:157103-14-5
Molecular Formula:C₂₅H₂₅Br₂NO₄
Molecular Weight:563.286
Hs Code.:
DSSTox Substance ID:DTXSID90935610
Nikkaji Number:J744.322F
Mol file:157103-14-5.mol

Synonyms:157103-14-5;Furo(2,3,4-cd)isoindole-2,6-dione, octahydro-4,5-dibromo-7-((4-methoxyphenyl)methyl)-3-methyl-7a-(phenylmethyl)-;C25H25Br2NO4;DTXSID90935610;C25-H25-Br2-N-O4;LS-70836;7a-Benzyl-4,5-dibromo-7-[(4-methoxyphenyl)methyl]-3-methyloctahydrofuro[2,3,4-cd]isoindole-2,6-dione;Octahydro-7a-benzyl-4,5-dibromo-3-methyl-7-(4-methoxybenzyl)furo[2,3,4-cd]isoindole-2,6-dione

Suppliers and Price of Furo(2,3,4-cd)isoindole-2,6-dione, octahydro-4,5-dibromo-7-((4-methoxyphenyl)methyl)-3-methyl-7a-(phenylmethyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of Furo(2,3,4-cd)isoindole-2,6-dione, octahydro-4,5-dibromo-7-((4-methoxyphenyl)methyl)-3-methyl-7a-(phenylmethyl)-

Chemical Property:

Vapor Pressure:3.1E-19mmHg at 25°C
Boiling Point:696.3°Cat760mmHg
Flash Point:374.9°C
Density:1.58g/cm³
XLogP3:5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:5
Exact Mass:563.01298
Heavy Atom Count:32
Complexity:736

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1C2C3C(C(C1Br)Br)C(=O)N(C3(OC2=O)CC4=CC=CC=C4)CC5=CC=C(C=C5)OC

Technology Process of Furo(2,3,4-cd)isoindole-2,6-dione, octahydro-4,5-dibromo-7-((4-methoxyphenyl)methyl)-3-methyl-7a-(phenylmethyl)-

There total 4 articles about Furo(2,3,4-cd)isoindole-2,6-dione, octahydro-4,5-dibromo-7-((4-methoxyphenyl)methyl)-3-methyl-7a-(phenylmethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 157103-13-4
3-benzyl-2,3,3a,4,5,7a-hexahydro-3-hydroxy-2-(4-methoxybenzyl)-5-methyl-1-oxo-1H-isoindole-4-carboxylic acid lactone

: 157103-14-5
3-benzyl-6,7-dibromo-2,3,3a,4,5,7a-hexahydro-3-hydroxy-2-(4-methoxybenzyl)-5-methyl-1-oxo-1H-isoindole-4-carboxylic acid lactone

Guidance literature:: With pyridine; pyridinium hydrobromide perbromide; In dichloromethane; for 1.5h; Yield given; Ambient temperature;

Reference yield:

: 100-44-7
benzyl chloride

: 157103-14-5
3-benzyl-6,7-dibromo-2,3,3a,4,5,7a-hexahydro-3-hydroxy-2-(4-methoxybenzyl)-5-methyl-1-oxo-1H-isoindole-4-carboxylic acid lactone

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Mg / 2.) Et₂O, THF, reflux, 8 h

2: pyridine hydrobromide perbromide, pyridine / CH₂Cl₂ / 1.5 h / Ambient temperature

With pyridine; pyridinium hydrobromide perbromide; magnesium; In dichloromethane;

Reference yield:

: 2393-23-9
4-methoxy-benzylamine

: 157103-14-5
3-benzyl-6,7-dibromo-2,3,3a,4,5,7a-hexahydro-3-hydroxy-2-(4-methoxybenzyl)-5-methyl-1-oxo-1H-isoindole-4-carboxylic acid lactone

Guidance literature:: Multi-step reaction with 3 steps

1: CH₂Cl₂ / 1.5 h / Heating

2: 1.) Mg / 2.) Et₂O, THF, reflux, 8 h

3: pyridine hydrobromide perbromide, pyridine / CH₂Cl₂ / 1.5 h / Ambient temperature

With pyridine; pyridinium hydrobromide perbromide; magnesium; In dichloromethane;