3-(methylsulfanyl)-6-phenylthieno[2,3-e][1,2,4]triazine

Base Information

• Chemical Name: 3-(methylsulfanyl)-6-phenylthieno[2,3-e][1,2,4]triazine
• CAS No.: 69347-03-1
• Molecular Formula: C12H9 N3 S2
• Molecular Weight: 259.35

Synonyms:NSC 299390

Chemical Property of 3-(methylsulfanyl)-6-phenylthieno[2,3-e][1,2,4]triazine

Chemical Property:

• Vapor Pressure: 7.41E-09mmHg at 25°C
• Boiling Point: 478.5°Cat760mmHg
• Flash Point: 243.2°C
• Density: 1.41g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-(methylsulfanyl)-6-phenylthieno[2,3-e][1,2,4]triazine

There total 13 articles about 3-(methylsulfanyl)-6-phenylthieno[2,3-e][1,2,4]triazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

3-Methylsulfanyl-6-(2-oxo-2-phenyl-ethyl)-4H-[1,2,4]triazin-5-one → 3-Methylsulfanyl-6-phenyl-thieno[2,3-e][1,2,4]triazine (69347-03-1)

Guidance literature:

With diphosphorus pentasulfide; In pyridine; for 6h; Heating;

Reference yield: 35.0%

4-amino-3-(methylthio)-6-styryl-1,2,4-triazin-5(4H)-one (22285-16-1) → 3-Methylsulfanyl-6-phenyl-thieno[2,3-e][1,2,4]triazine (69347-03-1) + 6-Phenyl-thieno[2,3-e][1,2,4]triazine-3-thiol (89569-78-8)

Guidance literature:

With diphosphorus pentasulfide; In pyridine; for 6h; Heating;

Reference yield: 30.0%

3-(methylthio)-6-styryl-1,2,4-triazin-5(2H)-one (35538-74-0) → 3-Methylsulfanyl-6-phenyl-thieno[2,3-e][1,2,4]triazine (69347-03-1)

Guidance literature:

With diphosphorus pentasulfide; In pyridine; for 6h; Heating;

upstream raw materials:

4-amino-3-(methylthio)-6-styryl-1,2,4-triazin-5(4H)-one

3-(methylthio)-6-styryl-1,2,4-triazin-5(2H)-one

6-Phenyl-thieno[2,3-e][1,2,4]triazine-3-thiol

methyl iodide

Downstream raw materials:

3-Morpholin-4-yl-6-phenyl-thieno[2,3-e][1,2,4]triazine

3-methanesulfonyl-6-phenylthieno[2,3-e][1,2,4]triazine

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