5-(3-Chlorophenyl)-3-(o-tolyl)-1H-1,2,4-triazole

Base Information

Chemical Name:5-(3-Chlorophenyl)-3-(o-tolyl)-1H-1,2,4-triazole
CAS No.:69095-76-7
Molecular Formula:C15H12ClN3
Molecular Weight:269.7289
Hs Code.:
Mol file:69095-76-7.mol

Synonyms:5-(m-Chlorophenyl)-3-(o-tolyl)-s-triazole;1H-1,2,4-Triazole,3-(3-chlorophenyl)-5-(2-methylphenyl);s-Triazole,5-(m-chlorophenyl)-3-(o-tolyl);

Suppliers and Price of 5-(3-Chlorophenyl)-3-(o-tolyl)-1H-1,2,4-triazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 5-(3-Chlorophenyl)-3-(o-tolyl)-1H-1,2,4-triazole

Chemical Property:

Vapor Pressure:1.44E-09mmHg at 25°C
Boiling Point:485.2°Cat760mmHg
Flash Point:279.3°C
PSA：41.57000
Density:1.266g/cm³
LogP:4.10050

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 5-(3-Chlorophenyl)-3-(o-tolyl)-1H-1,2,4-triazole

There total 5 articles about 5-(3-Chlorophenyl)-3-(o-tolyl)-1H-1,2,4-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 827-64-5,75782-97-7,75782-98-8
ethyl 3-chlorobenzenecarboximidate hydrochloride

: hydrazide of o-toluic acid

: 69095-76-7
3-(m-Chlorophenyl)-5-(o-tolyl)-1H-1,2,4-triazole

Guidance literature:: In cyclohexane; benzene;

Reference yield:

: 118-90-1
ortho-methylbenzoic acid

: 69095-76-7
5-(3-Chloro-phenyl)-3-o-tolyl-1H-[1,2,4]triazole

Guidance literature:: Multi-step reaction with 4 steps

1: SOCl₂ / 2 h / Heating

2: hydrazine hydrate / CH₂Cl₂; ethanol / 3 h / Ambient temperature

3: 1.) MeCN, reflux, 1 h, 2.) 110 deg C, 2 h

4: 0.17 h / 200 °C

With thionyl chloride; hydrazine hydrate; In ethanol; dichloromethane;
DOI:10.1021/jm00362a018

Reference yield:

: 933-88-0
ortho-toluoyl chloride

: 69095-76-7
5-(3-Chloro-phenyl)-3-o-tolyl-1H-[1,2,4]triazole

Guidance literature:: Multi-step reaction with 3 steps

1: hydrazine hydrate / CH₂Cl₂; ethanol / 3 h / Ambient temperature

2: 1.) MeCN, reflux, 1 h, 2.) 110 deg C, 2 h

3: 0.17 h / 200 °C

With hydrazine hydrate; In ethanol; dichloromethane;
DOI:10.1021/jm00362a018