Benzenamine, N-[(4,5-dimethoxy-2-nitrophenyl)methylene]-4-methyl-

Base Information

Chemical Name:Benzenamine, N-[(4,5-dimethoxy-2-nitrophenyl)methylene]-4-methyl-
CAS No.:18505-71-0
Molecular Formula:C16H16N2O4
Molecular Weight:300.314
Hs Code.:
DSSTox Substance ID:DTXSID30354689
Mol file:18505-71-0.mol

Synonyms:Benzenamine, N-[(4,5-dimethoxy-2-nitrophenyl)methylene]-4-methyl-;18505-71-0;DTXSID30354689;SR-01000198285;SR-01000198285-1

Suppliers and Price of Benzenamine, N-[(4,5-dimethoxy-2-nitrophenyl)methylene]-4-methyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Benzenamine, N-[(4,5-dimethoxy-2-nitrophenyl)methylene]-4-methyl-

Chemical Property:

XLogP3:3.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:4
Exact Mass:300.11100700
Heavy Atom Count:22
Complexity:388

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)N=CC2=CC(=C(C=C2[N+](=O)[O-])OC)OC

Technology Process of Benzenamine, N-[(4,5-dimethoxy-2-nitrophenyl)methylene]-4-methyl-

There total 3 articles about Benzenamine, N-[(4,5-dimethoxy-2-nitrophenyl)methylene]-4-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 20357-25-9
6-nitroveratraldehyde

: 106-49-0,12221-03-3
p-toluidine

: 18505-71-0
6-(p-tolylaminomethylidene)-3,4-dimethoxynitrobenzene

Guidance literature:: In ethanol; for 2h; Heating;
DOI:10.1016/S0040-4020(01)00166-1 DOI:10.1021/ol035049z

Reference yield:

: 120-14-9
3,4-dimethoxy-benzaldehyde

: 18505-71-0
6-(p-tolylaminomethylidene)-3,4-dimethoxynitrobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: nitric acid / 20 °C

2: ethanol / 0.5 h / Reflux

With nitric acid; In ethanol;
DOI:10.1016/j.tet.2010.07.048

Reference yield:

: 121-33-5,8014-42-4
vanillin

: 18505-71-0
6-(p-tolylaminomethylidene)-3,4-dimethoxynitrobenzene

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetone / 1.5 h / 20 °C / Reflux

2: nitric acid / 20 °C

3: ethanol / 0.5 h / Reflux

With nitric acid; potassium carbonate; In ethanol; acetone;
DOI:10.1016/j.tet.2010.07.048