N-(9,10-dioxo-9,10-dihydroanthracen-1-yl)-3-[2-(2-hydroxyethyl)piperidin-1-yl]propanamide hydrochloride (2:1)

Base Information

Chemical Name:N-(9,10-dioxo-9,10-dihydroanthracen-1-yl)-3-[2-(2-hydroxyethyl)piperidin-1-yl]propanamide hydrochloride (2:1)
CAS No.:112764-16-6
Molecular Formula:C₂₄H₂₆N₂O₄*ClH
Molecular Weight:442.942
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(9,10-dioxo-9,10-dihydroanthracen-1-yl)-3-[2-(2-hydroxyethyl)piperidin-1-yl]propanamide hydrochloride (2:1)

Chemical Property:

Vapor Pressure:6.24E-19mmHg at 25°C
Boiling Point:671.2°Cat760mmHg
Flash Point:359.7°C
Density:g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N-(9,10-dioxo-9,10-dihydroanthracen-1-yl)-3-[2-(2-hydroxyethyl)piperidin-1-yl]propanamide hydrochloride (2:1)

There total 2 articles about N-(9,10-dioxo-9,10-dihydroanthracen-1-yl)-3-[2-(2-hydroxyethyl)piperidin-1-yl]propanamide hydrochloride (2:1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1484-84-0
2(RS)-(2-hydroxyethyl)piperidine

: 20210-30-4
N-(9,10-dihydro-9,10-dioxo-1-anthracenyl)-3-chloropropanamide

: 112764-16-6
N-(9,10-dihydro-9,10-dioxo-1-anthracenyl)-2-(2-hydroxyethyl)-1-piperidinepropanamide hydrochloride

Guidance literature:: With hydrogenchloride; In ethanol; at 60 ℃; for 16h;
DOI:10.1021/jm00399a028

Reference yield:

: 82-45-1
1-amino-9,10-anthracenedione

: 112764-16-6
N-(9,10-dihydro-9,10-dioxo-1-anthracenyl)-2-(2-hydroxyethyl)-1-piperidinepropanamide hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / pyridine / toluene / 5 h / 60 °C

2: 74 percent / 2.) aq. HCl / ethanol / 16 h / 60 °C

With pyridine; hydrogenchloride; In ethanol; toluene;
DOI:10.1021/jm00399a028