Silane, (dithiodi-4,1-phenylene)bis[trimethyl-

Base Information

Chemical Name:Silane, (dithiodi-4,1-phenylene)bis[trimethyl-
CAS No.:18546-89-9
Molecular Formula:C18H26S2Si2
Molecular Weight:362.707
Hs Code.:
DSSTox Substance ID:DTXSID20463193
Nikkaji Number:J2.151.169B
Wikidata:Q82288022

Synonyms:Silane, (dithiodi-4,1-phenylene)bis[trimethyl-;18546-89-9;RNHDNEGPJOGBBX-UHFFFAOYSA-;DTXSID20463193;InChI=1/C18H26S2Si2/c1-21(2,3)17-11-7-15(8-12-17)19-20-16-9-13-18(14-10-16)22(4,5)6/h7-14H,1-6H3

Suppliers and Price of Silane, (dithiodi-4,1-phenylene)bis[trimethyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Silane, (dithiodi-4,1-phenylene)bis[trimethyl-

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:5
Exact Mass:362.10144625
Heavy Atom Count:22
Complexity:296

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C[Si](C)(C)C1=CC=C(C=C1)SSC2=CC=C(C=C2)[Si](C)(C)C

Technology Process of Silane, (dithiodi-4,1-phenylene)bis[trimethyl-

There total 3 articles about Silane, (dithiodi-4,1-phenylene)bis[trimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 22515-25-9
[4-(methylsulfanyl)phenyl]trimethylsilane

: 1295631-11-6
C₁₀H₁₅FSSi

: 1295631-13-8
C₁₀H₁₅FOSSi

: 1295631-14-9
C₂₀H₃₀S₂Si₂

: 54560-64-4
Methyl-4-trimethylsilylphenylsulfoxid

: 18546-89-9
bis-[(4-trimethylsilyl)phenyl]disulfide

Guidance literature:: With xenon difluoride; In Hexafluorobenzene; at 20 ℃; for 1h; Pyrex vessel;
DOI:10.1016/j.tet.2011.02.016

Reference yield:

: 17878-43-2
[4-(trimethylsilyl)phenyl]magnesium bromide

: 17882-12-1
4-trimethylsilylbenzenethiol

: 18546-89-9
bis-[(4-trimethylsilyl)phenyl]disulfide

Guidance literature:: With sulfur;

Reference yield:

: 104-95-0
(4-bromophenyl)thioanisole

: 1295631-11-6
C₁₀H₁₅FSSi

: 1295631-13-8
C₁₀H₁₅FOSSi

: 1295631-14-9
C₂₀H₃₀S₂Si₂

: 54560-64-4
Methyl-4-trimethylsilylphenylsulfoxid

: 18546-89-9
bis-[(4-trimethylsilyl)phenyl]disulfide

Guidance literature:: Multi-step reaction with 2 steps

1.1: iodine; magnesium; ethylene dibromide / diethyl ether

1.2: Reflux

2.1: xenon difluoride / Hexafluorobenzene / 1 h / 20 °C / Pyrex_.(R). vessel

With xenon difluoride; iodine; magnesium; ethylene dibromide; In Hexafluorobenzene; diethyl ether;
DOI:10.1016/j.tet.2011.02.016